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Please be aware that this old REACH registration data factsheet is no longer maintained; it remains frozen as of 19th May 2023.

The new ECHA CHEM database has been released by ECHA, and it now contains all REACH registration data. There are more details on the transition of ECHA's published data to ECHA CHEM here.

Diss Factsheets

Physical & Chemical properties

Boiling point

Currently viewing:

Administrative data

Endpoint:
boiling point
Type of information:
experimental study
Adequacy of study:
key study
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
guideline study

Data source

Reference
Reference Type:
study report
Title:
Unnamed
Year:
2018

Materials and methods

Test guidelineopen allclose all
Qualifier:
according to guideline
Guideline:
OECD Guideline 103 (Boiling Point)
Qualifier:
according to guideline
Guideline:
EU Method A.2 (Boiling Temperature)
GLP compliance:
yes (incl. QA statement)
Type of method:
differential scanning calorimetry

Test material

Constituent 1
Chemical structure
Reference substance name:
3,3'-oxydipropanol
EC Number:
219-251-4
EC Name:
3,3'-oxydipropanol
Cas Number:
2396-61-4
Molecular formula:
C6H14O3
IUPAC Name:
3-(3-hydroxypropoxy)propan-1-ol
Test material form:
liquid

Results and discussion

Boiling point
Key result
Atm. press.:
>= 1 002 - <= 1 007
Decomposition:
yes
Decomp. temp.:
>= 220 °C
Remarks on result:
other: Not detectable, because of thermal decomposition.

Any other information on results incl. tables

No thermal effect was observed up to 220 °C. In the temperature range of 220 °C up to 260 °C, an exothermic effect with an energy release of -360 J/g was detected. This effect was directly followed by a relatively broad endothermic signal in the temperature range of 260 °C up to 310 °C. Note that in both measurements more than 90 % of the sample got lost.

Table1:     Results of the DSC-measurements

No.

Sample weight / mg

Onset of Effect / °C

Range of effect / °C

Weight loss / mg

Atmospheric pressure / hPa(a)

Remark

PN16256

15.42

---
288.35

220 – 260 (exo)
260 – 310 (endo)

14.53

1006.6

Figure 2

PN16260

13.81

---
288.54

230 – 260 (exo)
260 – 310 (endo)

13.11

1001.9

Figure 3

No melting or boiling of the test item was observed up to 220 °C where the test item started to undergo an exothermic effect.

Applicant's summary and conclusion