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Please be aware that this old REACH registration data factsheet is no longer maintained; it remains frozen as of 19th May 2023.

The new ECHA CHEM database has been released by ECHA, and it now contains all REACH registration data. There are more details on the transition of ECHA's published data to ECHA CHEM here.

Diss Factsheets

Administrative data

Endpoint:
melting point/freezing point
Type of information:
experimental study
Adequacy of study:
key study
Study period:
Testing was conducted between 18 October 2010 and 17 December 2010.
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
other: see 'Remark'
Remarks:
Study conducted in compliance with agreed protocols, with no or minor deviations from standard test guidelines and/or minor methodological deficiencies, which do not affect the quality of the relevant results. The study report was conclusive, done to a valid guideline and the study was conducted under GLP conditions.

Data source

Reference
Reference Type:
study report
Title:
Unnamed
Year:
2010
Report date:
2011

Materials and methods

Test guideline
Qualifier:
according to guideline
Guideline:
OECD Guideline 102 (Melting point / Melting Range)
Deviations:
no
GLP compliance:
yes (incl. QA statement)
Type of method:
pour point

Test material

Constituent 1
Reference substance name:
Additiv 309
IUPAC Name:
Additiv 309
Details on test material:
Sponsor's identification: Additiv 309
Description : Brown liquid
Batch number : 651098135
Purity : Technical: Amine: >90% Oleylpropylenediamine(>98% Fatty acid diamine)
Water: max 0.5%
Distilled tall oil: >95% fatty acid
(ca. 5% unsaponifiables)
Date received : 03 September 2010
Expiry Date : 31 March 2012
Storage conditions: room temperature in the dark

Results and discussion

Melting / freezing point
Melting / freezing pt.:
< -17 °C
Decomposition:
no
Sublimation:
no
Remarks on result:
other: The pour point result above is +/- 3 deg C. No atmospheric pressure was recorded for this endpoint.

Any other information on results incl. tables

Results

The measured stationary points are shown in the following table.

Table 4.1

Measurement

Determination 1

Determination 2

Stationary point (°C)

-20

-20

Pour point (°C)

-17

-17

Mean pour point: -17 ± 3°C (256 ± 3 K)

Applicant's summary and conclusion

Conclusions:
The pour point of the test item has been determined to be -17 ± 3°C (256 ± 3 K).
Executive summary:

Method

The determination was carried out using the pour point method, BS 2000: Part 15 (equivalent to ISO 3016), designed to be compatible with Method 102 of the OECD Guidelines for Testing of Chemicals, 27 July 1995.

Conclusion

The pour point of the test item has been determined to be -17 ± 3°C (256 ± 3 K).