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Please be aware that this old REACH registration data factsheet is no longer maintained; it remains frozen as of 19th May 2023.

The new ECHA CHEM database has been released by ECHA, and it now contains all REACH registration data. There are more details on the transition of ECHA's published data to ECHA CHEM here.

Diss Factsheets

Physical & Chemical properties

Melting point / freezing point

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Administrative data

Link to relevant study record(s)

Reference
Endpoint:
melting point/freezing point
Type of information:
experimental study
Adequacy of study:
key study
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
guideline study
Justification for type of information:
Data is from experimental study report
Qualifier:
according to guideline
Guideline:
OECD Guideline 102 (Melting point / Melting Range)
GLP compliance:
no
Type of method:
other: Capillary / Metal block method
Key result
Melting / freezing pt.:
72.1 - 75.3 °C
Atm. press.:
969.3 hPa
Decomposition:
no
Sublimation:
no

  Method Details    Observations Remarks if, any
Guideline OECD 102    -
 Method  Capillary/metal block  -
 Principle of method  The temperature at which a solid becomes a liquid at standard atmospheric pressure  -
 Grinding of Test item done    Yes
 Atmospheric pressure hPa  969.3hPa 
 Decomposition  Decomposition temperature (°C), if applicable  No
 Sublimation  Sublimation temperature (°C), if applicable  No
 mean melting temperature range  °C  72.1 -75.3°C
Conclusions:
The melting point determination of test chemical was done following OECD Guideline 102 and according to the metal block capillary method. The test was conducted in replicates and mean melting temperature range was determined to be 72.1 -75.3°C at 969.3hPa.
Executive summary:

The melting point determination of test chemical was done as per the test guideline OECD 102. The method followed was according to Capillary/metal block. The mean melting temperature range was determined to be 72.1 -75.3°C at 969.3 hPa.

Description of key information

The melting point determination of test chemical was done as per the test guideline OECD 102. The method followed was according to Capillary/metal block. The mean melting temperature range was determined to be 72.1 -75.3°C at 969.3 hPa.

Key value for chemical safety assessment

Melting / freezing point at 101 325 Pa:
72.1 °C

Additional information

The melting point determination of test chemical was done as per the test guideline OECD 102. The method followed was according to Capillary/metal block. The mean melting temperature range was determined to be 72.1 -75.3°C at 969.3 hPa.

Based on the data obtained from reliable hand book and authoritative database,melting point of test chemical was observed to be in the range of 76.5 - 76.7 °C which was near to the kay value .