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Please be aware that this old REACH registration data factsheet is no longer maintained; it remains frozen as of 19th May 2023.

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Diss Factsheets

Physical & Chemical properties

Melting point / freezing point

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Administrative data

Link to relevant study record(s)

Reference
Endpoint:
melting point/freezing point
Type of information:
experimental study
Adequacy of study:
key study
Study period:
From 2020-02-13 to 2020-04-22
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
guideline study
Qualifier:
according to guideline
Guideline:
OECD Guideline 102 (Melting point / Melting Range)
Deviations:
no
Qualifier:
according to guideline
Guideline:
EU Method A.1 (Melting / Freezing Temperature)
Deviations:
no
GLP compliance:
yes (incl. QA statement)
Type of method:
differential scanning calorimetry
Key result
Melting / freezing pt.:
113.2 °C
Remarks on result:
other: Test item was a black to brownish solidified melt.

Three DSC measurements with a heating rate of 10 l/min showed an endothermal effect (melting) in the temperature range of 95 - 130°C. The onset temperature was derived from the intersection of the tangent line with the highest slope of the endothermal peak with the baseline and ranged from 112.90 to 113.61°C (Test item was a brownish solidified melt, no mass loss; Test item was a black solidified melt,mass loss: from 58% to 61%).

Conclusions:
The test item had a mean melting point of 113.2°C.
Executive summary:

The aim of the test was to determine the melting point of the test item according to the OECD 102 guideline/ A.1 method (Differential scanning calorimetry) and following GLP.

The test item had a mean melting point of 113.2°C.

Description of key information

Key value for chemical safety assessment

Melting / freezing point at 101 325 Pa:
113.2 °C

Additional information