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Physical & Chemical properties

Melting point / freezing point

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Administrative data

Link to relevant study record(s)

Reference
Endpoint:
melting point/freezing point
Type of information:
experimental study
Adequacy of study:
key study
Study period:
17 March 2015 to 22 May 2015
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
guideline study
Qualifier:
according to guideline
Guideline:
EU Method A.1 (Melting / Freezing Temperature)
Deviations:
no
Qualifier:
according to guideline
Guideline:
OECD Guideline 102 (Melting point / Melting Range)
Deviations:
no
GLP compliance:
yes (incl. QA statement)
Type of method:
pour point
Specific details on test material used for the study:
Purity: >95%; UVCB
Expiry Date: 31 January 2016
Key result
Melting / freezing pt.:
< -20 °C
Atm. press.:
ca. 101 325 Pa
Remarks on result:
other: The pour point was determined to be less than -20 ˚C (<253 K)

Starting at 46 ˚C and at intervals of 3 ˚C, the sample was tilted to a horizontal position for a period of 5 seconds, during which the sample was observed for signs of flow. The sample was continued to be observed until the temperature reached below -20 ˚C.

Conclusions:
The melting point of tall oil reaction products with diethylenetriamine has been determined to be less than -20 ˚C (<253 K)
Executive summary:

The melting point of the test item was determined using the pour point method according to the OECD guideline 102/EU Method A.1. The melting point of tall oil reaction products with diethylenetriamine was determined to be less than -20 ˚C (<253 K).

Description of key information

The melting point of tall oil reaction products with diethylenetriamine was determined to be less than -20 ˚C (<253 K) using the pour point method according to the OECD guideline 102/EU Method A.1.

Key value for chemical safety assessment

Melting / freezing point at 101 325 Pa:
-20 °C

Additional information