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Diss Factsheets

Physical & Chemical properties

Particle size distribution (Granulometry)

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Administrative data

Endpoint:
particle size distribution (granulometry)
Type of information:
experimental study
Adequacy of study:
key study
Study period:
August 27, 2002
Reliability:
2 (reliable with restrictions)
Rationale for reliability incl. deficiencies:
other: Valid method

Data source

Reference
Reference Type:
study report
Title:
Unnamed
Year:
2002
Report date:
2002

Materials and methods

Principles of method if other than guideline:
Malvern laser diffraction
Type of method:
Laser scattering/diffraction
Type of distribution:
volumetric distribution

Test material

Constituent 1
Chemical structure
Reference substance name:
2,2'-[(2,2',5,5'-tetrachloro[1,1'-biphenyl]-4,4'-diyl)bis(azo)]bis[N-(2,4-dimethylphenyl)-3-oxobutyramide]
EC Number:
244-776-0
EC Name:
2,2'-[(2,2',5,5'-tetrachloro[1,1'-biphenyl]-4,4'-diyl)bis(azo)]bis[N-(2,4-dimethylphenyl)-3-oxobutyramide]
Cas Number:
22094-93-5
Molecular formula:
C36H32Cl4N6O4
IUPAC Name:
2,2'-[(2,2',5,5'-tetrachlorobiphenyl-4,4'-diyl)didiazene-2,1-diyl]bis[N-(2,4-dimethylphenyl)-3-oxobutanamide]
Test material form:
solid: nanoform, no surface treatment

Results and discussion

Particle sizeopen allclose all
Percentile:
D50
Mean:
4 µm
Remarks on result:
other: Migrated from fields under 'Mass median diameter' as D50 percentile. No source field for Standard deviation.
Percentile:
D50
Mean:
4 µm
St. dev.:
0.52

Any other information on results incl. tables

The product contains about 10 weight-% fine dust below 1 µm not covered by the method of analysis.

Standard deviation calculated from experience with pigments: 0.13 x D50 (minimum value: 0.1)

Applicant's summary and conclusion

Conclusions:
The mass median diameter is 4 µm.
Executive summary:

The mass median diameter using Malvern laser diffraction (volumetric distribution) was determined to be 4 µm.