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Physical & Chemical properties

Particle size distribution (Granulometry)

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Reference
Endpoint:
particle size distribution (granulometry)
Type of information:
experimental study
Adequacy of study:
key study
Study period:
07/05/2016-07/05/2016
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
guideline study
Justification for type of information:
Experimental test result performed using standard test guidelines
Qualifier:
according to guideline
Guideline:
other: as mentioned below
Principles of method if other than guideline:
The particle size distribution of test item Dialuminium tris[2-(2,4,5,7-tetrabromo-6-oxido-3-oxoxanthen-9-yl)-3,4,5,6-tetrachlorobenzoate] (CAS No. 15876-58-1)was determined by granulometric analysis with rotap sieve shaker
GLP compliance:
no
Type of method:
sieving
Type of particle tested:
primary particle
Type of distribution:
mass based distribution
Specific details on test material used for the study:
- Name of test material : Dialuminium tris[2-(2,4,5,7-tetrabromo-6-oxido-3-oxoxanthen-9-yl)-3,4,5,6-tetrachlorobenzoate]
- Molecular formula:C20H4Br4Cl4O5 2/3Al
- Molecular weight : 2404.904 g/mol
- Smiles notation : C1=C2C(=C3C=C(C(=O)C(=C3OC2=C(C(=C1Br)[O-])Br)Br)Br)C4=C(C(=C(C(=C4Cl)Cl)Cl)Cl)C(=O)[O-].C1=C2C(=C3C=C(C(=O)C(=C3OC2=C(C(=C1Br)[O-])Br)Br)Br)C4=C(C(=C(C(=C4Cl)Cl)Cl)Cl)C(=O)[O-].C1=C2C(=C3C=C(C(=O)C(=C3OC2=C(C(=C1Br)[O-])Br)Br)Br)C4=C(C(=C(C(=C4Cl)Cl)Cl)Cl)C(=O)[O-].[Al+3].[Al+3]
- InChl : 1S/3C20H4Br4Cl4O5.2Al/c3*21-5-1-3-7(8-9(20(31)32)13(26)15(28)14(27)12(8)25)4-2-6(22)17(30)11(24)19(4)33-18(3)10(23)16(5)29;;/h3*1-2,29H,(H,31,32);;/q;;;2*+3/p-6
- Substance type : Organic
- Physical state: Solid
Key result
Percentile:
D50
Remarks on result:
other: Mass mean diameter
No.:
#1
Size:
150 µm
Distribution:
31.86 %
Remarks on result:
other: No other detail available
No.:
#2
Size:
106 µm
Distribution:
22.19 %
Remarks on result:
other: No other detail available
No.:
#3
Size:
75 µm
Distribution:
27.91 %
Remarks on result:
other: No other detail available
No.:
#4
Size:
53 µm
Distribution:
2 %
Remarks on result:
other: No other detail available
No.:
#5
Size:
25 µm
Distribution:
11.6 %
Remarks on result:
other: No other detail available
No.:
#6
Size:
10 µm
Distribution:
2.04 %
Remarks on result:
other: No other detail available

There was some loss of particles that remain adhered within the mesh of the finest sieve.

Sieve sizes(in microns)

Weight of petridishes (g)

Weight of petridishes +

test item (g)

Test item quantity retained after sieving (g)

Percentage (%) of test item*

150 microns

47.105

50.291

3.186

31.86 %

106 microns

44.102

46.321

2.219

22.19%

75 microns

45.217

48.008

2.791

27.91%

53 microns

43.712

43.912

0.200

2.00%

25 microns

37.941

39.101

1.160

11.60%

10 microns

38.414

38.210

0.204

2.04%

Conclusions:
The particle size distribution of test item Dialuminium tris[2-(2,4,5,7-tetrabromo-6-oxido-3-oxoxanthen-9-yl)-3,4,5,6-tetrachlorobenzoate] (CAS No. 15876-58-1) was determined by granulometric analysis with rotap sieve shaker. The particle size distribution was observed to be in the range of 150 micron to 10 micron.
Executive summary:

The particle size distribution of test item Dialuminium tris[2 -(2,4,5,7 -tetrabromo-6 -oxido-3 -oxoxanthen-9 -yl)-3,4,5,6 -tetrachlorobenzoate] (CAS No. 15876 -58 -1) was determined by granulometric analysis with rotap sieve shaker. The particle size distribution was observed to be in the range of 150 micron to 10 micron.

Description of key information

The particle size distribution of test item Dialuminium tris[2-(2,4,5,7-tetrabromo-6-oxido-3-oxoxanthen-9-yl)-3,4,5,6-tetrachlorobenzoate] (CAS No. 15876-58-1) was determined by granulometric analysis with rotap sieve shaker. The particle size distribution was observed to be in the range of 150 micron to 10 micron.

Additional information

The particle size distribution of test item Dialuminium tris[2-(2,4,5,7-tetrabromo-6-oxido-3-oxoxanthen-9-yl)-3,4,5,6-tetrachlorobenzoate] (CAS No. 15876-58-1) was determined by granulometric analysis with rotap sieve shaker. The particle size distribution was observed to be in the range of 150 micron to 10 micron.