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Diss Factsheets

Physical & Chemical properties

Melting point / freezing point

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Administrative data

Link to relevant study record(s)

Referenceopen allclose all

Endpoint:
melting point/freezing point
Type of information:
experimental study
Adequacy of study:
supporting study
Study period:
08 Jul 2011
Reliability:
2 (reliable with restrictions)
Rationale for reliability incl. deficiencies:
guideline study without detailed documentation
Qualifier:
according to guideline
Guideline:
OECD Guideline 102 (Melting point / Melting Range)
GLP compliance:
no
Type of method:
method to determine freezing temperature
Melting / freezing pt.:
< -20 °C
Atm. press.:
ca. 1 013 hPa
Remarks on result:
other: pour point

There are no values given for pressure but assumed to be measured at normal pressure (1013 hPa). No information is given on specification on decomposition/sublimation temperature.

Endpoint:
melting point/freezing point
Type of information:
experimental study
Adequacy of study:
supporting study
Reliability:
2 (reliable with restrictions)
Rationale for reliability incl. deficiencies:
data from handbook or collection of data
Principles of method if other than guideline:
Handbook data, no information is given on test method

GLP compliance:
no
Type of method:
other: not specified
Melting / freezing pt.:
-31 °C
Atm. press.:
ca. 1 013 hPa

There are no values given for pressure but assumed to be measured at normal pressure (1013 hPa). Published data, no information is given on specification on decomposition/sublimation temperature.

Endpoint:
melting point/freezing point
Type of information:
experimental study
Adequacy of study:
key study
Study period:
11 May 2011
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
comparable to guideline study
Qualifier:
according to guideline
Guideline:
other: ASTM D 97-02
Principles of method if other than guideline:
ASTM D 97-02 : ”Standard Test Method for Pour Point of Petroleum Oils”
GLP compliance:
no
Other quality assurance:
other: ISO 9001:2008
Type of method:
pour point
Melting / freezing pt.:
-78 °C
Atm. press.:
1 013 hPa

Results:

Pour Point of Reference substance

Analysis N°

Pour – Point

[°C]

1

-24

2

-24

3

-24

Mean

-24

Pour Point of EGDA

Analysis N°

Pour – Point

[°C]

1

-78

2

-78

3

-78

Mean

-78

Endpoint:
melting point/freezing point
Type of information:
experimental study
Adequacy of study:
supporting study
Reliability:
2 (reliable with restrictions)
Rationale for reliability incl. deficiencies:
data from handbook or collection of data
GLP compliance:
not specified
Type of method:
other: not specified
Melting / freezing pt.:
-31 °C
Atm. press.:
ca. 1 013 hPa

There are no values given for pressure but assumed to be measured at normal pressure (1013 hPa). Published data, no information given on specification of decomposition/sublimation temperature.

Endpoint:
melting point/freezing point
Type of information:
experimental study
Adequacy of study:
supporting study
Reliability:
2 (reliable with restrictions)
Rationale for reliability incl. deficiencies:
data from handbook or collection of data
Remarks:
SPARC database match
Principles of method if other than guideline:
database data, no information is given on test method
GLP compliance:
not specified
Type of method:
other: not specified
Melting / freezing pt.:
-31 °C
Atm. press.:
ca. 1 013 hPa

There are no values given for pressure but assumed to be measured at normal pressure (1013 hPa). Published data, no information given on specification of decomposition/sublimation temperature.

Description of key information

pour point: -78 °C at ca. 1013 hPa (Pour point tester, ASTM D 97 -02)

Key value for chemical safety assessment

Melting / freezing point at 101 325 Pa:
-78 °C

Additional information

The other values reported within other experiment (< -20 °C) and literature (-31 °C) are supporting.