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Please be aware that this old REACH registration data factsheet is no longer maintained; it remains frozen as of 19th May 2023.

The new ECHA CHEM database has been released by ECHA, and it now contains all REACH registration data. There are more details on the transition of ECHA's published data to ECHA CHEM here.

Diss Factsheets

Administrative data

Endpoint:
relative density
Type of information:
experimental study
Adequacy of study:
key study
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
guideline study

Data source

Reference
Reference Type:
study report
Title:
Unnamed
Year:
2013
Report date:
2013

Materials and methods

Test guideline
Qualifier:
according to guideline
Guideline:
OECD Guideline 109 (Density of Liquids and Solids)
GLP compliance:
yes (incl. QA statement)
Type of method:
pycnometer method

Test material

Constituent 1
Chemical structure
Reference substance name:
bis(N,N,N-trimethyladamantan-1-aminium) sulfate
EC Number:
600-024-7
Cas Number:
1000777-61-6
Molecular formula:
C26 H48 N2 O4 S
IUPAC Name:
bis(N,N,N-trimethyladamantan-1-aminium) sulfate
Test material form:
other: granular
Details on test material:
Name of test material (as cited in study report): Tricyclo[3.3.1.13,7]decan-1-aminium, N,N,N,-trimethyl-, sulfate (2:1)
Analytical purity: 83.2 g/100g (by 1H NMR spectrometry; study no 11 L00496)
Lot/batch No.: ADTAS P5310.10.10
Expiration date of the lot/batch: Oct 20, 2011

Results and discussion

Density
Type:
relative density
Density:
1.24
Temp.:
20 °C

Any other information on results incl. tables

Results:

    1st determination 2nd determination
A Mass of pycnometer empty
(corrected for air)
39.6044 36.9902 cm3
B Mass of pycnometer with test item
(corrected for air)
50.0404 51.0658
C Mass of pycnometer with test item and
displacement liquid
63.0948 61.3213
D Mass of displacement liquid calculated for
the total pycnometer volume
19.7411 19.7791
E Mass of test item (B - A) 10.4359 14.0756
F Mass of displacement liquid (C - B) 13.0544 14.0756
G Mass of displacement liquid calculated for
the volume taken by the test item (D - F)
6.6866 9.5236
H Density of the test item
(E/G * density of displacement liquid)
1.2378 g/cm3  1.2326 g/cm3
I Relative density D204(H/density of water
at 4°C)
mean: 1.24

Masses are listed in gram. Results are calculated from not rounded single values.

The estimated accuracy is ± 0.01

Applicant's summary and conclusion