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Please be aware that this old REACH registration data factsheet is no longer maintained; it remains frozen as of 19th May 2023.

The new ECHA CHEM database has been released by ECHA, and it now contains all REACH registration data. There are more details on the transition of ECHA's published data to ECHA CHEM here.

Diss Factsheets

Administrative data

Endpoint:
melting point/freezing point
Type of information:
experimental study
Adequacy of study:
key study
Study period:
April 17, 2007 - May 31, 2007
Reliability:
1 (reliable without restriction)
Cross-reference
Reason / purpose for cross-reference:
reference to same study

Data source

Reference
Reference Type:
study report
Title:
Unnamed
Year:
2007
Report date:
2007

Materials and methods

Test guidelineopen allclose all
Qualifier:
according to guideline
Guideline:
OECD Guideline 102 (Melting point / Melting Range)
Version / remarks:
, 1995
Deviations:
no
Qualifier:
according to guideline
Guideline:
EU Method A.1 (Melting / Freezing Temperature)
Version / remarks:
, 1992
Deviations:
no
GLP compliance:
yes (incl. QA statement)
Remarks:
signed 2004-09-06
Type of method:
thermal analysis
Remarks:
Differential Scanning Calorimetry

Test material

Reference
Name:
Unnamed
Type:
Constituent
Type:
Constituent
Details on test material:
- Name of test material (as cited in study report): Symrose; (cis/trans) 4-(3-methylbutyl)cyclohexanol
- Substance type: technical product
- Physical state: liquid, colourless
- Storage condition of test material: ambient temperature

Results and discussion

Melting / freezing point
Melting / freezing pt.:
-21 °C
Atm. press.:
ca. 113 mBar

Any other information on results incl. tables

Two DSC-runs in aluminium crucibles with a hole showed an endothermic effect in the temperature range of -30 to 5 °C with an onset temperature of -21 °C.

Table 1: Melting Point

Ident-No.

Onset / °C

Temperature range / °C

Crucible

25829

-21.34

-30 to 5 °C

Aluminium with a whole

25840

-21.02

-30 to 5 °C

Aluminium with a whole

Applicant's summary and conclusion

Conclusions:
Maximum accuracy of melting point +/- 0.5 °C