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The new ECHA CHEM database has been released by ECHA, and it now contains all REACH registration data. There are more details on the transition of ECHA's published data to ECHA CHEM here.

Diss Factsheets

Physical & Chemical properties

Melting point / freezing point

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Administrative data

Link to relevant study record(s)

Referenceopen allclose all

Endpoint:
melting point/freezing point
Type of information:
other: Publication
Adequacy of study:
weight of evidence
Study period:
1955
Reliability:
3 (not reliable)
Rationale for reliability incl. deficiencies:
other: Data obtained from a publication on the toxicity of the test item.
Principles of method if other than guideline:
Guideline not specified; data from publication.
GLP compliance:
not specified
Type of method:
other: not specified; data from handbook or collection of data.
Melting / freezing pt.:
>= 35.5 - <= 36 °C
Remarks on result:
other: Atmospheric pressure not reported in publication.
Conclusions:
According to the publication "Comparative Toxicity of Boranes" published by Levinskas G.J., the melting point of dimethylamine-borane (1:1) is in the range of 35.5 - 36 °C.
Executive summary:

According to the publication "Comparative Toxicity of Boranes" published by Levinskas G.J., the melting point of dimethylamine-borane (1:1) is in the range of 35.5 - 36 °C.

Endpoint:
melting point/freezing point
Type of information:
other: Data from handbook or collection of data.
Adequacy of study:
weight of evidence
Study period:
1959
Reliability:
2 (reliable with restrictions)
Rationale for reliability incl. deficiencies:
data from handbook or collection of data
Principles of method if other than guideline:
Guideline not specified; data from handbook or collection of data.
GLP compliance:
not specified
Type of method:
other: not specified; data from handbook or collection of data.
Melting / freezing pt.:
37 °C
Remarks on result:
other: Atmospheric pressure not reported in data collection.
Conclusions:
According to the data collection "Beiträge zur Chemie des Bors, I: Darstellung und Eigenschaften der Alkylamin-borane, R(3-n)H(n)*BH3" published by H. Noeth & H. Beyer in 1960, the melting point of dimethylamine-borane (1:1) is 37 °C.
Executive summary:

According to the data collection "Beiträge zur Chemie des Bors, I: Darstellung und Eigenschaften der Alkylamin-borane, R(3-n)H(n)*BH3" published by H. Noeth & H. Beyer in 1960, the melting point of dimethylamine-borane (1:1) is 37°C.

Endpoint:
melting point/freezing point
Type of information:
other: Experimental value from database.
Adequacy of study:
weight of evidence
Study period:
not reported
Reliability:
2 (reliable with restrictions)
Rationale for reliability incl. deficiencies:
data from handbook or collection of data
Principles of method if other than guideline:
Guideline not specified; data obtained from database (collection of data);
GLP compliance:
not specified
Type of method:
other: Data obtained from database (collection of data).
Melting / freezing pt.:
36 °C
Remarks on result:
other: Atmospheric pressure not reported in database.
Conclusions:
According to the SRC PhysProp Database the melting point of dimethylamine-borane (1:1) is 36 °C. The value was determined experimentally and is also on file in EPA's EPI Suite.
Executive summary:

According to the SRC PhysProp Database the melting point of dimethylamine-borane (1:1) is 36 °C. The value was determined experimentally and is also on file in EPA's EPI Suite.

Description of key information

The melting point of the substance dimethylamine-borane (1:1) was evaluated in a weight-of-evidence approach using two literature references and one database entry. The melting point values obtained by these sources are in very good accordance and therefore sufficient for assessment of this endpoint. The mean melting point value is approximately 36 °C. The single values from the different sources are as follows:

- Levinskas J.G., 1955. Comparative Toxicity of Boranes: 35.5 - 36 °C;

- Noeth H. & Beyer H., 1960. Beiträge zur Chemie des Bors, I: Darstellung und Eigenschaften der Alkylamin-borane, R(3 -n)H(n)*BH3: 37 °C;

- Experimental value from SRC's PhysProp Database bundled with EPA's EpiSuite: 36 °C.

Key value for chemical safety assessment

Melting / freezing point at 101 325 Pa:
36 °C

Additional information