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Please be aware that this old REACH registration data factsheet is no longer maintained; it remains frozen as of 19th May 2023.

The new ECHA CHEM database has been released by ECHA, and it now contains all REACH registration data. There are more details on the transition of ECHA's published data to ECHA CHEM here.

Diss Factsheets

Administrative data

Endpoint:
melting point/freezing point
Type of information:
experimental study
Adequacy of study:
key study
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
guideline study

Data source

Reference
Reference Type:
study report
Title:
Unnamed
Report date:
2022

Materials and methods

Test guidelineopen allclose all
Qualifier:
according to guideline
Guideline:
OECD Guideline 102 (Melting point / Melting Range)
Version / remarks:
27 July 1995
Deviations:
no
Qualifier:
according to guideline
Guideline:
EU Method A.1 (Melting / Freezing Temperature)
Version / remarks:
No. 440/2008 of 30 May 2008
Deviations:
no
GLP compliance:
yes
Type of method:
differential scanning calorimetry

Test material

Constituent 1
Reference substance name:
Reaction mass of benzoyl chloride, toluoyl chloride and 2-methyl resorcinol
Molecular formula:
not applicable
IUPAC Name:
Reaction mass of benzoyl chloride, toluoyl chloride and 2-methyl resorcinol
Test material form:
solid: particulate/powder
Details on test material:
Appearance: beige powder

Results and discussion

Melting / freezing point
Key result
Melting / freezing pt.:
> 99 - < 107 °C

Any other information on results incl. tables

The thermograms and thermographic data for Determinations 1 and 2 are shown in the
following table and figures below:


Table 2 Thermographic Data































 


Thermal Event



 


Interpretation



Temperature (°C)



Determination 1



Determination 2



 


Broad endotherm



Start of melting



~ 99



~ 99



Peak of melting



105.8



105.5



End of melting



~ 107



~ 107



Mean result: Melted over the range approximately 99 to 107 °C (372 to 380 K)

Applicant's summary and conclusion

Conclusions:
The test item has been determined to melt over the range approximately 99 to 107 °C (372 to 380 K).