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Physical & Chemical properties

Boiling point

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Administrative data

Link to relevant study record(s)

Reference
Endpoint:
boiling point
Type of information:
experimental study
Adequacy of study:
key study
Study period:
Experimental starting date: 03 January 2017 Experimental completion date: 10 June 2017
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
guideline study
Qualifier:
according to guideline
Guideline:
EU Method A.2 (Boiling Temperature)
Deviations:
no
Qualifier:
according to guideline
Guideline:
OECD Guideline 103 (Boiling Point)
Deviations:
no
GLP compliance:
yes (incl. QA statement)
Type of method:
differential scanning calorimetry
Specific details on test material used for the study:
Appearance/Physical state: Amber colored gelatinous solid
Batch: E00268-014-212
Purity: 100%
Expiry date: 10 June 2018
Storage conditions: Room temperature in the dark
Sampling conditions: Heating to 50 to 80 °C was utilized to enable sampling of test item for some tests.
Key result
Decomposition:
yes
Remarks:
The boiling point obtained from determinations 9 and 10, showed a clear endotherm at approximately 390 °C, losses of approximately 100%, leaving a residue of black shiny stain. The boiling can therefore be concluded to occur during decomposition.
Decomp. temp.:
>= 310 °C
Remarks on result:
other: Boiling with decomposition from 310 °C (583 K) at 99.4 to 102.5 kPa
Remarks:
The boiling point results, obtained from determinations 9 and 10, showed a clear endotherm at approximately 390 °C, losses of approximately 100%, leaving a residue of black shiny stain. The boiling can therefore be concluded to occur during decomposition. Boiling with decomposition from 310 °C (583 K) at 99.4 to 102.5 kPa.

Please see attached Thermogram's & Table 2 Thermographic Data

Conclusions:
The Boiling point was: Boiling with decomposition from 310 °C (583 K), at 99.4 to 102.5 kPa,
Executive summary:

Boiling Point. Boiling with decomposition from 310 °C (583 K), at 99.4 to 102.5 kPa, by differential scanning calorimetry, designed to be compatible with Method A.2 Boiling Temperature of Commission Regulation (EC) No 440/2008 of 30 May 2008 and Method 103 of the OECD Guidelines for Testing of Chemicals, 27 July 1995. As the test item decomposed, no value for boiling point could be determined.

Description of key information

The Boiling point was:  Boiling with decomposition from 310 °C (583 K), at 99.4 to 102.5 kPa, therefore as the test item decomposed, no value for boiling point could be determined.

Key value for chemical safety assessment

Additional information

Boiling Point. Boiling with decomposition from 310 °C (583 K), at 99.4 to 102.5 kPa, by differential scanning calorimetry, designed to be compatible with Method A.2 Boiling Temperature of Commission Regulation (EC) No 440/2008 of 30 May 2008 and Method 103 of the OECD Guidelines for Testing of Chemicals, 27 July 1995. As the test item decomposed, no value for boiling point could be determined.