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Please be aware that this old REACH registration data factsheet is no longer maintained; it remains frozen as of 19th May 2023.

The new ECHA CHEM database has been released by ECHA, and it now contains all REACH registration data. There are more details on the transition of ECHA's published data to ECHA CHEM here.

Diss Factsheets

Physical & Chemical properties

Melting point / freezing point

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Administrative data

Link to relevant study record(s)

Reference
Endpoint:
melting point/freezing point
Type of information:
experimental study
Adequacy of study:
key study
Study period:
02 Jun to 18 Jul 2017
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
guideline study
Qualifier:
according to guideline
Guideline:
OECD Guideline 102 (Melting point / Melting Range)
Qualifier:
equivalent or similar to guideline
Guideline:
EU Method A.1 (Melting / Freezing Temperature)
GLP compliance:
not specified
Type of method:
differential scanning calorimetry
Remarks on result:
not determinable
Remarks:
A transition in physical form from a hard waxy solid to a soft gel occurs between temperatures of -37 °C and 12 °C

The test item shows a melting area of crystalline subcomponents between -37 °C and 12 °C according to the definition in the OECD Guideline 102 (mean value from repeat determination).

-36 °C to 11 °C (from first measurement)

-36 °C to 11 °C (from second measurement)

-39 °C to 14 °C (from third measurement)

At temperatures of about -57 °C the test item shows a glass transition temperature.

The first cooling run shows a crystallization.

The melting area (of crystalline subcomponents) describes a transition in physical form from a hard waxy solid to a soft gel.

Description of key information

A transition in physical form from a hard waxy solid to a soft gel occurs between temperatures of -37 °C and 12 °C (OECD 102, DSC method)

Key value for chemical safety assessment

Additional information