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Please be aware that this old REACH registration data factsheet is no longer maintained; it remains frozen as of 19th May 2023.

The new ECHA CHEM database has been released by ECHA, and it now contains all REACH registration data. There are more details on the transition of ECHA's published data to ECHA CHEM here.

Diss Factsheets

Administrative data

Endpoint:
melting point/freezing point
Type of information:
experimental study
Adequacy of study:
key study
Study period:
February 13, 2017 to March 03, 2017
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
guideline study

Data source

Reference
Reference Type:
study report
Title:
Unnamed
Year:
2017
Report date:
2017

Materials and methods

Test guideline
Qualifier:
according to guideline
Guideline:
OECD Guideline 102 (Melting point / Melting Range)
Deviations:
no
GLP compliance:
yes (incl. QA statement)
Type of method:
other: capillary tube in a metal block

Test material

Constituent 1
Chemical structure
Reference substance name:
rel-(3S,5aR,7aR,11aR,11bS)-3,8,8,11a-tetramethyldodecahydro-5H-3,5aepoxynaphtho[2,1-c]oxepine
Molecular formula:
C18H30O2
IUPAC Name:
rel-(3S,5aR,7aR,11aR,11bS)-3,8,8,11a-tetramethyldodecahydro-5H-3,5aepoxynaphtho[2,1-c]oxepine
Constituent 2
Chemical structure
Reference substance name:
rel-(3R,5aS,7aR,11aR,11bS)-3,8,8,11a-tetramethyldodecahydro-5H-3,5aepoxynaphtho[2,1-c]oxepine
Cas Number:
220432-47-3
Molecular formula:
C18H30O2
IUPAC Name:
rel-(3R,5aS,7aR,11aR,11bS)-3,8,8,11a-tetramethyldodecahydro-5H-3,5aepoxynaphtho[2,1-c]oxepine
Specific details on test material used for the study:
SOURCE OF TEST MATERIAL
Lot No.: VE00464199
Purity: 99.9 % (major peak)
Expiration date: April 17, 2017

Results and discussion

Melting / freezing point
Key result
Melting / freezing pt.:
117 °C
Atm. press.:
1 013 hPa
Decomposition:
no
Sublimation:
no

Applicant's summary and conclusion

Conclusions:
From the tests described above, it can be concluded that the melting point of Amberketal is (values rounded off): 390 K (117°C)
Executive summary:

The melting point of Amberketal was measured according to OECD Guideline No. 102 (capillary tube in a metal block). The result can be expressed as follows (values rounded off): The melting point of Amberketal:390 K (117°C).