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Diss Factsheets

Administrative data

Endpoint:
auto-ignition temperature (liquids)
Type of information:
experimental study
Adequacy of study:
key study
Study period:
October 10, 2016 to November 09, 2016
Reliability:
2 (reliable with restrictions)
Rationale for reliability incl. deficiencies:
guideline study with acceptable restrictions

Data source

Reference
Reference Type:
study report
Title:
Unnamed
Year:
2016
Report date:
2016

Materials and methods

Test guidelineopen allclose all
Qualifier:
according to guideline
Guideline:
EU Method A.15 (Auto-Ignition Temperature (Liquids and Gases))
Deviations:
no
Qualifier:
according to guideline
Guideline:
DIN 51794 (Testing of mineral oil hydrocarbons - Determination of ignition temperature)
Deviations:
no
GLP compliance:
no

Test material

Constituent 1
Chemical structure
Reference substance name:
7,11-dimethyldodeca-4,6,10-trien-3-one
EC Number:
247-878-3
EC Name:
7,11-dimethyldodeca-4,6,10-trien-3-one
Cas Number:
26651-96-7
Molecular formula:
C14H22O
IUPAC Name:
(4E,6E)-7,11-dimethyldodeca-4,6,10-trien-3-one
impurity 1
Chemical structure
Reference substance name:
3,6,10-trimethylundeca-3,5,9-trien-2-one
EC Number:
214-245-8
EC Name:
3,6,10-trimethylundeca-3,5,9-trien-2-one
Cas Number:
1117-41-5
Molecular formula:
C14H22O
IUPAC Name:
3,6,10-trimethylundeca-3,5,9-trien-2-one
Test material form:
liquid
Specific details on test material used for the study:
Lot No.: SC00018390
Aspect: yellow liquid
Purity: 89.1% 7,11-dimethyldodeca-4,6,10-trien-3-one (sum of the isomers)
6.4% 3,6,10-trimethylundeca-3,5,9-trien-2-one (sum of the isomers)

Results and discussion

Auto-ignition temperature (liquids / gases)
Key result
Auto-ignition temperature:
245 °C
Remarks on result:
other: +/- 10ºC

Any other information on results incl. tables

The lowest temperature giving a positive effect was 249ºC

The injected volume was 100ul, the ignition delay was 47s. At a temperature of 244ºC no ignition was observed. Therefore, after rounding-off to the next-lower multiple of 5ºC:

Auto-ignition temperature of Pseudoisoraldeine A: 245 +/- 10ºC

Applicant's summary and conclusion

Conclusions:
The lowest temperature giving a positive effect was 249ºC
The injected volume was 100ul, the ignition delay was 47s. At a temperature of 244ºC no ignition was observed. Therefore, after rounding-off to the next-lower multiple of 5ºC:
Auto-ignition temperature of Pseudoisoraldeine A: 245 +/- 10ºC
Executive summary:

Auto-ignition temperature of Pseudoisoraldeine A: 245 +/- 10ºC