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Diss Factsheets

Administrative data

Endpoint:
relative self-ignition temperature (solids)
Type of information:
experimental study
Adequacy of study:
key study
Study period:
27/01/2011
Reliability:
2 (reliable with restrictions)
Rationale for reliability incl. deficiencies:
study well documented, meets generally accepted scientific principles, acceptable for assessment
Justification for type of information:
The test was performed using a vertical tube apparatus manufactured by Chilworth Technology Limited and a capacitive spark. The test is based on IEC 61241-2-3.
Minimum Ignition Temperature - Cloud:
The test was performed using the vertical (Godbert-Greenwald) furnace. Dust is dispersed by a pulse of compressed air into the top of the cylindrical furnace core. Observations are made at the base exit from the core to determine ignition. The test is performed in accordance with IEC Standard 61241-2-1, Part 2.

Data source

Reference
Reference Type:
study report
Title:
Unnamed
Year:
2011
Report date:
2011

Materials and methods

Test guideline
Qualifier:
no guideline followed
Principles of method if other than guideline:
Total inductance : < 25 μH (Capacitive method, without inductance)
Test Temp. : 20°C
Preparation : Sample tested ground then sieved < 63 μm

Minimum Ignition Temperature - Cloud
The test was performed using the vertical (Godbert-Greenwald) furnace. Dust is dispersed by a pulse of compressed air into the top of the cylindrical furnace core. Observations are made at the base exit from the core to determine ignition. The test is performed in accordance with IEC Standard 61241-2-1, Part 2.
GLP compliance:
yes

Test material

Constituent 1
Chemical structure
Reference substance name:
2,2-dimethylpropanethioamide
EC Number:
677-829-5
Cas Number:
630-22-8
Molecular formula:
C5H11NS
IUPAC Name:
2,2-dimethylpropanethioamide
Test material form:
solid: crystalline
Details on test material:
Purity or Composition 100.0 %

Results and discussion

Relative self-ignition temperature (solids)
Key result
Relative self-ignition temperature:
> 400 °C

Applicant's summary and conclusion

Conclusions:
Thermal Stability Characterisation
Layer (5 mm layer) Ignition Temperature (“LIT”, °C) > 400
Minimum Ignition Energy (“MIE”, mJ) 15 - 17

Minimum (dust cloud) Ignition Temperature (“MIT”, °C) 340