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Diss Factsheets

Physical & Chemical properties

Density

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Link to relevant study record(s)

Reference
Endpoint:
density, other
Remarks:
relative density
Type of information:
experimental study
Adequacy of study:
key study
Study period:
2019-07-30 to 2019-08-01
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
guideline study
Reason / purpose for cross-reference:
reference to same study
Reason / purpose for cross-reference:
reference to same study
Qualifier:
according to guideline
Guideline:
OECD Guideline 109 (Density of Liquids and Solids)
Deviations:
no
GLP compliance:
yes (incl. QA statement)
Type of method:
pycnometer method
Specific details on test material used for the study:
- Appearance: solid at room temperature
Type:
density
Density:
3.457 other: g/mL
Temp.:
20 °C
Remarks on result:
other: relative density: d(20,4) = 3.457

Raw data of the determination

W1: Weight of the pycnometer with air: 23.4388 g / 24.6666 g

W2: Weight of the pycnometer filled with deionized water: 48.3764 g / 49.3137 g

W3: Weight of the pycnometer filled with displacement liquid: 40.5166 g / 41.5452 g

W4: Weight of the pycnometer half-filled with the sample: 37.5431 g / 40.6381 g

W5: Weight of the pycnometer filled with sample and displacement liquid: 51.8338 g / 54.3611 g

Literature data (CRC Handbook of Chemistry and Physics 75th Edition):

d (20, w) (density of water at 20 °C) = 0.9982 g/mL

d (4, w) (density of water at 4 °C) = 0.99997 g/mL

d (20, a) (density of air at 20 °C) = 0.0012 g/mL

displacement liquid: n-heptan

Calculation of the relative density with correction of buoyancy due to the air

Corrected density of displacement liquid (d) at 20°C

d(20,d) = (W3 –W1/ W2 –W1)· [d(20,w) – d(20,a)] + d(20,a)

d1(20,d) = 0.6840 g/mL d2(20,d) = 0.6840 g/mL

Corrected density of solid at 20°C

d(20,S) = [W4 – W1 / (W4 – W1 + W3 –W5)]· [d(20,d) – d(20,a)] + d(20,a)

d1(20,S) = 3.4564 g/mL d2(20,S) = 3.4568 g/mL

Corrected relative density of solid

d(20,4,S) = d(20,S) / d(4, w)

d1(20,4,S) = 3.4565 d2(20,4,S) = 3.4570

mean value of 2 determinations: d(20,4,S) = 3.457

Conclusions:
The test item Lithium titanate has a relative density at 20 °C compared to water at 4 °C of 3.457.

Description of key information

The test item Lithium titanate has a relative density at 20 °C compared to water at 4 °C of 3.457.

Key value for chemical safety assessment

Relative density at 20C:
3.457

Additional information