Registration Dossier
Registration Dossier
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EC number: 265-352-1 | CAS number: 65060-02-8
Boiling point
Administrative data
Link to relevant study record(s)
- Endpoint:
- boiling point
- Type of information:
- experimental study
- Adequacy of study:
- key study
- Study period:
- From October 19, 2016 to November 11, 2016
- Reliability:
- 1 (reliable without restriction)
- Rationale for reliability incl. deficiencies:
- guideline study
- Qualifier:
- according to guideline
- Guideline:
- OECD Guideline 103 (Boiling Point)
- Deviations:
- no
- Qualifier:
- according to guideline
- Guideline:
- EU Method A.2 (Boiling Temperature)
- Deviations:
- no
- GLP compliance:
- not specified
- Type of method:
- differential scanning calorimetry
- Key result
- Boiling pt.:
- ca. 304 °C
- Atm. press.:
- 1 007 mBar
- Decomposition:
- yes
- Decomp. temp.:
- > 304 °C
- Remarks on result:
- other: thermal decomposition with evaporation of the decomposition components
- Conclusions:
- Under the study conditions, the boiling and/or thermal decomposition of the test substance was determined to be earliest at ca. 304°C (at 1007 mbar).
- Executive summary:
A study was conducted to determine the boiling point of the test substance, C16 TMA-MS (93.44% active), according to OECD Guideline 103 and EU Method A.2. To determine the boiling behaviour (three independent single measurements), the test substance was measured by Differential Scanning Calorimetry (DSC) between 5°C and 400°C with a heating rate of 10 K/min. For the measurement; a partially capsulated crucible was used. From 304°C the test substance showed a boiling and/or thermal decomposition with evaporation of the decomposition components. Under the study conditions, the boiling and/or thermal decomposition of the test substance was determined to be earliest at ca. 304°C (at 1007 mbar) (Henkel, 2016).
Reference
Results
- Determination following 3 independent single measurements:
305°C (from first measurement)
303°C (from second measurement)
304°C (from third measurement)
- From 304°C the test substance showed a boiling and/or thermal decomposition with evaporation of the decomposition components. The DSC measurements were confirmed by means of TGA measurements under the same measuring conditions. The start of the area of boiling temperatures was defined by using the on-set temperature.
Description of key information
The boiling point of the test substance was determined using differential scanning calorimetry, according to OECD Guideline 103 and EU Method A.2 (Henkel, 2016).
Key value for chemical safety assessment
Additional information
The test substance was determined to be earliest at ca. 304°C (at 1007 mbar).
Information on Registered Substances comes from registration dossiers which have been assigned a registration number. The assignment of a registration number does however not guarantee that the information in the dossier is correct or that the dossier is compliant with Regulation (EC) No 1907/2006 (the REACH Regulation). This information has not been reviewed or verified by the Agency or any other authority. The content is subject to change without prior notice.
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