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Please be aware that this old REACH registration data factsheet is no longer maintained; it remains frozen as of 19th May 2023.

The new ECHA CHEM database has been released by ECHA, and it now contains all REACH registration data. There are more details on the transition of ECHA's published data to ECHA CHEM here.

Diss Factsheets

Administrative data

Endpoint:
melting point/freezing point
Type of information:
experimental study
Adequacy of study:
key study
Study period:
2012
Reliability:
2 (reliable with restrictions)
Rationale for reliability incl. deficiencies:
other: according to valid method (DSC)

Data source

Reference
Reference Type:
study report
Title:
Unnamed
Year:
2012
Report date:
2012

Materials and methods

Principles of method if other than guideline:
Differential Scanning Calorimetry
GLP compliance:
not specified
Type of method:
thermal analysis

Test material

Constituent 1
Chemical structure
Reference substance name:
3-amino-4-chlorobenzamide
EC Number:
243-231-4
EC Name:
3-amino-4-chlorobenzamide
Cas Number:
19694-10-1
Molecular formula:
C7H7ClN2O
IUPAC Name:
3-amino-4-chlorobenzamide

Results and discussion

Melting / freezing point
Melting / freezing pt.:
162 °C
Atm. press.:
ca. 1 atm
Decomposition:
yes
Decomp. temp.:
>= 306 °C
Remarks on result:
other: A second endothermic peak apears at 278°C. An exothermic decomposition starts at 306°C. Because of the overlap of endothermic and exothermic processes, the energy measured for the exothermic process (234 J/g) is less than the true decomposition energy

Applicant's summary and conclusion

Conclusions:
The tested melting point is 162°C.
Executive summary:

The melting point was determined using a Differential Scanning Calorimeter.