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Diss Factsheets

Physical & Chemical properties

Density

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Administrative data

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Reference
Endpoint:
relative density
Type of information:
experimental study
Adequacy of study:
key study
Study period:
From 30 November 2021 to 11 March 2022
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
guideline study
Qualifier:
according to guideline
Guideline:
OECD Guideline 109 (Density of Liquids and Solids)
Version / remarks:
2012
Deviations:
no
Qualifier:
according to guideline
Guideline:
EU Method A.3 (Relative Density)
Version / remarks:
2008
Deviations:
no
GLP compliance:
yes (incl. QA statement)
Type of method:
pycnometer method
Specific details on test material used for the study:
Actual storage conditions: Stored in original plastic bag in a ventilated closed cupboard at normal laboratory temperature.
Dynamic viscosity of test material:
not relevant (solid)
Key result
Type:
relative density
Density:
0.373 other: The relative density has no dimension.
Temp.:
20 °C
Type:
density
Density:
372.9 kg/m³
Temp.:
20 °C




Results of the three determinations are reported in the following table:















































Determination123
m0 (g)31.4390731.6196931.14173
m1 (g)81.491181.644581.2637
m2 (g)81.491781.644781.2639
m3 (g)33.9458934.9141134.48477
m4 (g)77.2983776.1085575.29161
Density ρe (g/ml)0.373470.372400.37015





The density obtained for each determination is close enough to respect validation criteria (difference below 1%).






Determinations 1 and 2 have the closest results (0.29% of difference). Their arithmetic mean is 372.9 kg/m3 at 20.0 +/- 0.1°C. The corresponding relative density of the test item is D20/4 = 0.373


As the results obtained with the pycnometer were found unusually low and as the substance is difficult to handle, a short tapped density test (non-GLP) was performed with the raw substance to compare results. A similar value (0.37 g/ml) was obtained and confirms the results obtained with the pycnometer method.













Conclusions:
The substance is much less dense than water.
Executive summary:



The density of the test substance was measured according OECD 109 / EU A3 guideline, pycnometer method (with aqueous saturated solution as displacement liquid), and under GLP .
Calibration was performed with water. Experiment was performed at 20 °C in triplicate, and the mean density was calculated from the two closest results. It was converted to relative density vs water at 4°C.


The density of the test substance at 20°C was 372.9 kg/m3. The relative density D20/4 was 0.373.




Description of key information




Density = 372.9 kg/m3 at 20°C. Relative density D20/4 = 0.373. The substance is much less dense than water. (OECD 109, pycnometer with displacement liquid, GLP; Noel Y., 2022)




Key value for chemical safety assessment

Relative density at 20C:
0.373

Additional information