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Reference
Endpoint:
relative self-ignition temperature (solids)
Type of information:
experimental study
Adequacy of study:
key study
Study period:
26 February 2018 - 27 March 2018
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
guideline study
Qualifier:
according to guideline
Guideline:
EU Method A.16 (Relative Self-Ignition Temperature for Solids)
GLP compliance:
yes (incl. QA statement)
Specific details on test material used for the study:
Appearance/Physical state: White powder
Batch: J1624Z
Purity: 94.9%
Storage conditions: Room temperature in the dark
Key result
Relative self-ignition temperature:
> 400 °C
Remarks on result:
no self ignition observed under the test conditions
Conclusions:
The test item has been determined to not have a relative self-ignition temperature below 400 °C.

Description of key information

Whilst heating the test item, no relevant exothermic reaction /self-heating of the sample has been observed. On completion of the test, the test item was a shrunken black charred mass.

The test item has been determined to not have a relative self-ignition temperature below 400 °C.

Key value for chemical safety assessment

Additional information

The determination was carried out using a procedure designed to be compatible with Method A.16 Relative Self-Ignition Temperature for Solids of Commission Regulation (EC) No 440/2008 of 30 May 2008.

The cube was completely filled with the test item and placed in the center of the oven at room temperature. A thermocouple was placed in the center of the sample and another in the oven. The oven temperature was programmed to increase from ambient to 400 °C at a rate of 0.5 °C/min. The temperature/time curves relating to the condition in the centre of the sample and the oven were recorded on a data logger. Before and after the test the appearance of the test item was recorded.