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Please be aware that this old REACH registration data factsheet is no longer maintained; it remains frozen as of 19th May 2023.

The new ECHA CHEM database has been released by ECHA, and it now contains all REACH registration data. There are more details on the transition of ECHA's published data to ECHA CHEM here.

Diss Factsheets

Administrative data

Endpoint:
melting point/freezing point
Type of information:
experimental study
Adequacy of study:
key study
Study period:
2017-04-12
Reliability:
2 (reliable with restrictions)
Rationale for reliability incl. deficiencies:
study well documented, meets generally accepted scientific principles, acceptable for assessment

Data source

Reference
Reference Type:
study report
Title:
Unnamed
Year:
2017
Report date:
2017

Materials and methods

Test guideline
Qualifier:
no guideline followed
Principles of method if other than guideline:
Determination of the melting point by the thermoanalytical technique DSC
GLP compliance:
no
Type of method:
differential scanning calorimetry

Test material

1
Chemical structure
Reference substance name:
Cobalt, [29H,31H-phthalocyaninato(2-)-N29,N30,N31,N32]-, sulfonated, sodium salts
EC Number:
290-971-9
EC Name:
Cobalt, [29H,31H-phthalocyaninato(2-)-N29,N30,N31,N32]-, sulfonated, sodium salts
Cas Number:
90294-83-0
Molecular formula:
CoC32H16-τN8(SO3Na)τ
IUPAC Name:
Cobalt, [29H,31H-phthalocyaninato(2-)-N29,N30,N31,N32]-, sulfonated, sodium salts
Test material form:
solid: particulate/powder

Results and discussion

Melting / freezing pointopen allclose all
Key result
Melting / freezing pt.:
>= 39.63 - <= 222.28 °C
Remarks on result:
other:
Remarks:
peak at 139.57°C
Key result
Melting / freezing pt.:
>= 260.53 - <= 289.36 °C
Remarks on result:
other:
Remarks:
peak at 260.53°C

Applicant's summary and conclusion

Conclusions:
The DSC shows an endothermic peak which covers a wide range between 39°C and 222°C, with a peak at 139°C.
Executive summary:

A determination of the thermal stability of the test item by DSC (Differential Scanning Calorimetry) was performed with a DSC Mettler TOLEDO DSC 1, using a perforated crucible.

The DSC shows an endothermic peak which covers a wide range between 39°C and 222°C, with a peak at 139°C. This endothermic peak is considerably broad, over 180°C. It does not seems to be melting point. It might be a relaxation phenomena due to the evaporation of water.