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Physical & Chemical properties

Boiling point

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Reference
Endpoint:
boiling point
Type of information:
experimental study
Adequacy of study:
key study
Study period:
07 July 2017 to 11 July 2017
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
guideline study
Qualifier:
according to guideline
Guideline:
OECD Guideline 103 (Boiling Point)
Version / remarks:
1995
Deviations:
no
Qualifier:
according to guideline
Guideline:
EU Method A.2 (Boiling Temperature)
Deviations:
no
Qualifier:
according to guideline
Guideline:
EPA OPPTS 830.7220 (Boiling Point / Boiling Range)
Version / remarks:
1996
Deviations:
no
GLP compliance:
yes (incl. QA statement)
Type of method:
differential scanning calorimetry
Key result
Atm. press.:
>= 995 - <= 1 005 hPa
Decomposition:
yes
Decomp. temp.:
250 °C
Remarks on result:
other: The test material has no boiling point up to the decomposition temperature.

- During the heating phase, no thermal effects were observed in the temperature range from -25 to 250 °C. It can be assumed that the test material has no boiling point in this temperature range, i.e. the test material has no boiling point up to a temperature of 250 °C.

-At approx. 250 °C the test material started to decompose. At approx. 350 °C the exothermic effect ended and an endothermic effect started. The reason for this effect is that some of the decomposition products of the test material start to boil. The endothermic effect ended at approx. 470 °C.

- No further thermal effects were observed up to the test end temperature of 500 °C.

Conclusions:
Under the conditions of this study, the test material has no boiling point up to the decomposition temperature of 250 °C at atmospheric pressure (995 – 1005 hPa).
Executive summary:

The boiling point of the test material was investigated in accordance with the standardised guidelines OECD 103, EU Method A.2 and EPA OCSPP 830.7220, under GLP conditions using differential scanning calorimetry.

During the heating phase, no thermal effects were observed in the temperature range from -25 to 250 °C. It can be assumed that the test material has no boiling point in this temperature range, i.e. the test material has no boiling point up to a temperature of 250 °C. At approx. 250 °C the test material started to decompose. At approx. 350 °C the exothermic effect ended and an endothermic effect started. The reason for this effect is that some of the decomposition products of the test material start to boil. The endothermic effect ended at approx. 470 °C. No further thermal effects were observed up to the test end temperature of 500 °C.

Under the conditions of this study, the test material has no boiling point up to the decomposition temperature of 250 °C at atmospheric pressure (995 – 1005 hPa).

Description of key information

Under the conditions of this study, the test material has no boiling point up to the decomposition temperature of 250 °C at atmospheric pressure (995 – 1005 hPa).

Key value for chemical safety assessment

Additional information

The boiling point of the test material was investigated in accordance with the standardised guidelines OECD 103, EU Method A.2 and EPA OCSPP 830.7220, under GLP conditions using differential scanning calorimetry. The study was awarded a reliability score of 1 in accordance with the criteria set forth by Klimisch et al. (1997).

During the heating phase, no thermal effects were observed in the temperature range from -25 to 250 °C. It can be assumed that the test material has no boiling point in this temperature range, i.e. the test material has no boiling point up to a temperature of 250 °C. At approx. 250 °C the test material started to decompose. At approx. 350 °C the exothermic effect ended and an endothermic effect started. The reason for this effect is that some of the decomposition products of the test material start to boil. The endothermic effect ended at approx. 470 °C. No further thermal effects were observed up to the test end temperature of 500 °C.

Under the conditions of this study, the test material has no boiling point up to the decomposition temperature of 250 °C at atmospheric pressure (995 – 1005 hPa).