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Please be aware that this old REACH registration data factsheet is no longer maintained; it remains frozen as of 19th May 2023.

The new ECHA CHEM database has been released by ECHA, and it now contains all REACH registration data. There are more details on the transition of ECHA's published data to ECHA CHEM here.

Diss Factsheets

Physical & Chemical properties

Melting point / freezing point

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Administrative data

Link to relevant study record(s)

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Endpoint:
melting point/freezing point
Type of information:
experimental study
Adequacy of study:
key study
Reliability:
2 (reliable with restrictions)
Rationale for reliability incl. deficiencies:
other: company data
Justification for type of information:
Company specification data which is considered reliable. May not have been tested according to GLP.
Qualifier:
equivalent or similar to guideline
Guideline:
OECD Guideline 102 (Melting point / Melting Range)
GLP compliance:
no
Type of method:
method to determine freezing temperature
Specific details on test material used for the study:
Purity > 90%
Key result
Melting / freezing pt.:
< -20 °C
Atm. press.:
101.3 kPa
Remarks on result:
other: assume standard atmospheric pressure

The sample remained a free-flowing liquid after being stored at -20.5 deg C for 24 hours.

Conclusions:
The freezing point of the distilled substance (purity > 99.3%) is less than -20 °C.
Endpoint:
melting point/freezing point
Type of information:
experimental study
Adequacy of study:
key study
Reliability:
2 (reliable with restrictions)
Rationale for reliability incl. deficiencies:
other: company data
Justification for type of information:
Company specification data which is considered reliable. May not have been tested according to GLP.
Qualifier:
equivalent or similar to guideline
Guideline:
OECD Guideline 102 (Melting point / Melting Range)
GLP compliance:
no
Type of method:
method to determine freezing temperature
Specific details on test material used for the study:
Purity >99%
Key result
Melting / freezing pt.:
< -20 °C
Atm. press.:
101.3 kPa
Remarks on result:
other: assume standard atmospheric pressure

The samples of the crude material remained free-flowing liquid after being stored at -20.5 deg C for 24 hours.

Conclusions:
The freezing point of the substance (purity > 99%) is less than -20 °C.

Description of key information

Less than -20 °C.

Key value for chemical safety assessment

Melting / freezing point at 101 325 Pa:
-20 °C

Additional information

The experimental freezing points of both the distilled and crude/undistilled substance are less than -20 °C.