Registration Dossier
Registration Dossier
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EC number: 212-042-9 | CAS number: 754-05-2
Flash point
Administrative data
- Endpoint:
- flash point, other
- Remarks:
- liquid
- Type of information:
- experimental study
- Adequacy of study:
- key study
- Study period:
- 2017
- Reliability:
- 2 (reliable with restrictions)
- Rationale for reliability incl. deficiencies:
- test procedure in accordance with national standard methods with acceptable restrictions
Data source
Reference
- Reference Type:
- study report
- Title:
- Unnamed
- Year:
- 2 017
- Report date:
- 2017
Materials and methods
Test guideline
- Qualifier:
- according to guideline
- Guideline:
- other: Method A of ASTM D3828
- GLP compliance:
- no
- Other quality assurance:
- other: not specified
- Type of method:
- closed cup
- Flash point apparatus:
- other: Rapid Tester (Model RT-1)
Test material
- Reference substance name:
- Trimethylvinylsilane
- EC Number:
- 212-042-9
- EC Name:
- Trimethylvinylsilane
- Cas Number:
- 754-05-2
- Molecular formula:
- C5H12Si
- IUPAC Name:
- trimethylvinylsilane
Constituent 1
- Specific details on test material used for the study:
- Lot# M3M02DMV, 99.57% pure
Results and discussion
Flash point
- Key result
- Flash point:
- <= -30 °C
- Atm. press.:
- other: not specified
- Remarks on result:
- other: unit not specified in the report
Any other information on results incl. tables
Iterative testing was used to identify a flash/no flash result at -20, -25 and -30°C. In each case, a flash was detected. The lower limit of the method and instrument is -30°C, so no further attempts were made at lower temperatures. Since we cannot confirm if the material will flash below -30°C, we report that the actual value at or below -30°C.
Applicant's summary and conclusion
- Executive summary:
The flash point of vinyltrimethylsilane (Lot# M3M02DMV, 99.57% pure) was determined using a Closed Cup Flashpoint Rapid Tester (Model RT-1) in accordance with Method A of ASTM D3828 (Standard Test Methods for Flash Point by Small Scale Closed Cup Tester) using a 2mL sample volume. The sample cup was cooled to at least 5°C below each target temperature using liquid nitrogen, was then allowed to reach equilibrium, and then was allowed to warm to the target temperature without added heat. The syringe and sample were cooled to at least 10°C below the test temperature by immersion in a sand bath that was cooled with liquid nitrogen.
Iterative testing was used to identify a flash/no flash result at -20, -25 and -30°C. In each case, a flash was detected. The lower limit of the method and instrument is -30°C, so no further attempts were made at lower temperatures. Since we cannot confirm if the material will flash below -30°C, we report that the actual value at or below -30°C.
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