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Administrative data

Endpoint:
melting point/freezing point
Type of information:
experimental study
Adequacy of study:
key study
Study period:
02 March 2015-19 June 2015
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
other: GLP-compliant study in accordance with EC A.1, OECD 102 and EPA OPPTS 830.7200.
Cross-reference
Reason / purpose for cross-reference:
reference to same study

Data source

Reference
Reference Type:
study report
Title:
Unnamed
Year:
2015
Report date:
2015

Materials and methods

Test guidelineopen allclose all
Qualifier:
according to guideline
Guideline:
EU Method A.1 (Melting / Freezing Temperature)
Version / remarks:
(2008)
Deviations:
no
Qualifier:
according to guideline
Guideline:
OECD Guideline 102 (Melting point / Melting Range)
Version / remarks:
(1995)
Deviations:
no
Qualifier:
according to guideline
Guideline:
EPA OPPTS 830.7200 (Melting Point / Melting Range)
Version / remarks:
(1998)
Deviations:
no
GLP compliance:
yes
Type of method:
thermal analysis
Remarks:
(differential scanning calorimetry)

Test material

Constituent 1
Chemical structure
Reference substance name:
3-[3-(1,1,1,3,5,5,5-heptamethyltrisiloxan-3-yl)propoxy]propane-1,2-diol
EC Number:
807-413-2
Cas Number:
70280-68-1
Molecular formula:
C13H34O5Si3
IUPAC Name:
3-[3-(1,1,1,3,5,5,5-heptamethyltrisiloxan-3-yl)propoxy]propane-1,2-diol
Test material form:
other: liquid
Details on test material:
- Name (as cited in study report): X-22-1927
- Appearance: clear light yellow liquid
- Storage conditions: at room temperature

Results and discussion

Melting / freezing pointopen allclose all
Melting / freezing pt.:
< -90 °C
Remarks on result:
other: Result from DSC Experiment 1.
Melting / freezing pt.:
< -80 °C
Remarks on result:
other: Result from 'Storage experiment in freezers'.

Any other information on results incl. tables

The test substance was observed to be a viscous liquid after storage at -21.8 ± 0.3°C and a very viscous liquid after storage at -81.6 ± 1.8°C.

Applicant's summary and conclusion

Conclusions:
The freezing temperature of X-22-1927 is < -80°C.