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Melting point / freezing point

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Reference
Endpoint:
melting point/freezing point
Type of information:
experimental study
Adequacy of study:
key study
Study period:
11/02/2015
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
guideline study
Justification for type of information:
Experimental test result performed using standard test guidelines
Qualifier:
according to guideline
Guideline:
other: as mention below
Principles of method if other than guideline:
freezing temeparature is measured
GLP compliance:
no
Type of method:
other: standard laboratory method
Specific details on test material used for the study:
- Name of test material (IUPAC name): 4-(5,5,6-trimethylbicyclo[2.2.1]hept-2-yl)cyclohexan-1-ol
- Molecular formula: C16H28O
- Molecular weight: 236.396 g/mol
- Smiles notation: OC1CCC([C@@H]2[C@@H]3C[C@@H](C(C)(C)[C@@H]3C)C2)CC1
- InChl: 1S/C16H28O/c1-10-14-8-12(16(10,2)3)9-15(14)11-4-6-13(17)7-5-11/h10-15,17H,4-9H2,1-3H3
- Substance type: Organic
- Physical state: liquid
Key result
Melting / freezing pt.:
< -10.3 °C
Atm. press.:
982.1 hPa
Decomposition:
no
Sublimation:
no
Remarks on result:
other: other details not available

Observation Table & Result :

 Method Details    Observations
 Guideline  -  
 Method Freezing Temperature Method  
 Principle of method

 The freezing point of a pure sample is

the temperature at which transition from liquid to

solid state takes place at atmospheric pressure.

 

Quantity of test item used

ml/g

 1 ml

 Type of cooling bath used

  1. Cold Water
  2. Crushed Ice
  3. Crushed Ice-Salt
  4. Dry Ice
  5. Other (specify)

 

Crushed Ice-

Salt

Type and model no. of temperature sensor used

  1. Glass thermometer
  2. Thermocouple
  3. Thermistor
  4. Other (specify)

Glass

thermometer

Atmospheric pressure

hPa

 982.1 hPa

 Freezing point °C

 °C

 less than -10.3°C

Conclusions:
Freezing point of test chemical was determine to be less than -10.3 Deg C at pressure 982.1 hPa.
Executive summary:

Freezing point of test chemical was determine to be less than -10.3 Deg C at pressure 982.1 hPa.

Description of key information

Freezing point of test chemical was determine to be less than -10.3 Deg C at pressure 982.1 hPa.

Key value for chemical safety assessment

Melting / freezing point at 101 325 Pa:
-10.3 °C

Additional information

Freezing point of test chemical was determine to be less than -10.3 Deg C at pressure 982.1 hPa.