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Physical & Chemical properties

Boiling point

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Administrative data

Link to relevant study record(s)

Reference
Endpoint:
boiling point
Type of information:
experimental study
Adequacy of study:
key study
Study period:
2012
Reliability:
1 (reliable without restriction)
Qualifier:
according to guideline
Guideline:
EU Method A.2 (Boiling Temperature)
Deviations:
no
Principles of method if other than guideline:
Standard Test Method for the Thermal Stability of Chemicals by Differential
Scanning Calorimetry’ - ASTM 537.02, referred to in Methods A1 and A2
GLP compliance:
yes (incl. QA statement)
Type of method:
differential scanning calorimetry
Boiling pt.:
218.93 °C
Atm. press.:
1 005.6 hPa

The DSC runs described below were carried out in sealed, high pressure stainless steel capsules at a heating rate of 10°C/minute, over the range 30° to 400°C, in a test chamber environment of Nitrogen at a purge rate of approximately 20ml/minute.

Two determinations of the onset temperature, for the distinct endotherm exhibited in each case (i.e. the boiling point), were carried out, with the following results:

 Sample

Reference

 Analysis Date  Boiling Point (°C)    
(a)   (b)  Av.    
 C630/12/0894  21 January 2013  219.95  218.91  218.93
Conclusions:
The boiling point of TBS at 1005.6 hPa was 218.93 0C
Executive summary:

The boiling point of TBS at 1005.6 hPa was 218.93 0C

Description of key information

The boiling point was 218.93° C when measured using EU Method A2.

Key value for chemical safety assessment

Boiling point at 101 325 Pa:
218.93 °C

Additional information