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Diss Factsheets

Physical & Chemical properties

Boiling point

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Administrative data

Link to relevant study record(s)

Reference
Endpoint:
boiling point
Type of information:
experimental study
Adequacy of study:
key study
Study period:
From November 04, 2015 to November 17, 2015
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
guideline study
Qualifier:
according to guideline
Guideline:
OECD Guideline 103 (Boiling point/boiling range)
Deviations:
no
Qualifier:
equivalent or similar to guideline
Guideline:
EU Method A.2 (Boiling Temperature)
Deviations:
no
GLP compliance:
not specified
Type of method:
differential scanning calorimetry
Specific details on test material used for the study:
Batch no.: RE 10-7
Key result
Atm. press.:
1 020 mBar
Decomposition:
yes
Decomp. temp.:
>= 80 - <= 200 °C
Remarks on result:
other: the test substance did not show boiling up to a temperature of 219°C

At 219°C, the test substance showed a beginning of an exothermic effect. The exothermic effect was recorded in the 1stheating run from two independent single measurements, at 221°C (from first measurement) and 217°C (from second measurement). Between approximately 80°C and 200°C, the test substance showed a boiling and/or thermal decomposition with evaporation of the decomposition components of a part component (approximately 7.2 weight % according to TGA measurements). The DSC measurements were confirmed by means of TGA measurements under the same measuring conditions.

Conclusions:
Under the study conditions, the substance did not show boiling up to 219°C at 1,020 mbar.
Executive summary:

A study was conducted to determine the boiling point of the substance according to OECD Guideline 103. The boiling point was measured between 5°C and 500°C with a heating rate of 1 K/min according to differential scanning calorimetry. For the measurement, a partially capsulated crucible was used. At 219°C, the test substance showed a beginning of an exothermic effect. The exothermic effect was recorded in the first run from two independent single measurements, at 221°C and at 217°C from the second run. Between approximately 80°C and 200°C, the test substance showed a boiling and/or thermal decomposition with evaporation of the decomposition components. The DSC measurements were confirmed by means of thermogravimetric analysis under the same conditions. Under the study conditions, the substance did not show boiling of the main component up to 219°C at 1,020 mbar (Kintrup, 2015).

Description of key information

The boiling point was determined according to OECD Guideline 103 (Kintrup, 2015) 

Key value for chemical safety assessment

Additional information

No boiling of the substance at temperatures up to 219°C at 1020 mbar.