Registration Dossier

Administrative data

Endpoint:
melting point/freezing point
Type of information:
experimental study
Adequacy of study:
key study
Study period:
14.02.2002
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
other: Guideline study

Data source

Reference
Reference Type:
study report
Title:
Unnamed
Year:
2002
Report Date:
2002

Materials and methods

Test guideline
Qualifier:
according to
Guideline:
EU Method A.1 (Melting / Freezing Temperature)
Deviations:
no
GLP compliance:
yes (incl. certificate)
Type of method:
thermal analysis

Test material

Reference
Name:
Unnamed
Type:
Constituent
Details on test material:
Batch 63B001
Purity 95.9 %

Results and discussion

Melting / freezing point
Key result
Decomposition:
yes
Decomp. temp.:
>= 200 - <= 540 °C
Sublimation:
no

Any other information on results incl. tables

No melting peak (endothermic reaction) in DSC was observed.

Between 200 °C and 540 °C the DSC showed exothermic peaks with different intensity, which indicated further decomposition of the test substance. A loss of mass began at about 290 °C. At 540 °C about 98 % of the initial mass was lost.

Applicant's summary and conclusion

Conclusions:
A melting point cannot be determined.