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Physical & Chemical properties

Melting point / freezing point

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Reference
Endpoint:
melting point/freezing point
Type of information:
experimental study
Adequacy of study:
key study
Study period:
2012-03-28 to 2012-08-06
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
other: The study has been performed according to OECD guideline 102 and EU method A.1 in a GLP certified testing facility.
Qualifier:
according to guideline
Guideline:
OECD Guideline 102 (Melting point / Melting Range)
Deviations:
no
Qualifier:
according to guideline
Guideline:
EU Method A.1 (Melting / Freezing Temperature)
Deviations:
no
GLP compliance:
yes (incl. QA statement)
Type of method:
capillary method
Key result
Melting / freezing pt.:
>= -44.1 - <= -40.4 °C
Atm. press.:
101.325 kPa
Decomposition:
no
Sublimation:
no

Table 2     Values Main Study

Melting point/range

Begin

End

First Determination

- 44.0 °C (229.2 K)

- 40.2 °C (233.0 K)

Second Determination

- 44.1 °C (229.1 K)

- 40.6 °C (232.6 K)

Conclusions:
The melting range was determined as -44.1°C to -40.4 °C (corresponding to 229.2 – 232.8 K).
Executive summary:

The determination of the melting point of 400112 has been performed according to OECD guideline 102 and EU method A.1 in a GLP certified testing facility. In both determinations, a melting range was detected. The melting range was determined as -44.1°C to -40.4 °C (corresponding to 229.2-232.8 K). These values are the means of two independent determinations.

All validity criteria were met. No observations were made which might cause doubts on the validity of the study outcome. Therefore, the result of the study is considered valid.

Description of key information

The melting range was determined as -44.1°C to -40.4 °C (corresponding to 229.2-232.8 K). These values are the means of two independent determinations.

Key value for chemical safety assessment

Additional information

The determination of the melting point of 400112 was performed according to OECD guideline 102 and EU method A.1 in a GLP-certified testing facility. In both determinations a melting range was detected. The melting range was determined as -44.1°C to -40.4 °C (corresponding to 229.2-232.8 K). These values are the means of two independent determinations.

All validity criteria were met. No observations were made which might cause doubts on the validity of the study outcome. Therefore, the result of the study is considered valid.