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The new ECHA CHEM database has been released by ECHA, and it now contains all REACH registration data. There are more details on the transition of ECHA's published data to ECHA CHEM here.

Diss Factsheets

Physical & Chemical properties

Melting point / freezing point

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Endpoint:
melting point/freezing point
Type of information:
experimental study
Adequacy of study:
key study
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
other: GLP guideline study
Qualifier:
according to guideline
Guideline:
OECD Guideline 102 (Melting point / Melting Range)
Principles of method if other than guideline:
The melting temperature was measured by Differential
Scanning Calorimetry.
GLP compliance:
yes (incl. QA statement)
Type of method:
thermal analysis
Decomposition:
yes
Decomp. temp.:
> 250 °C

No melting point found below 400 °C. No melting point was found between -50°C and decomposition

of the test item. The test item is solid at room temperature.

Observed thermic processes:

A broad endothermic peak was observed between about 100°C

and 200°C. This can be interpreted as a loss of volatile

components. After the run the test item was visual unchanged.

To survey the thermic behaviour of the test item the

measurement was run up to 400°C. Exothermic decomposition

was observed at about 250°C. After the run the test

item was not melted.

Endpoint:
melting point/freezing point
Type of information:
read-across from supporting substance (structural analogue or surrogate)
Adequacy of study:
key study
Justification for type of information:
The analogue approach is appropriate for fulfilling the data requirement as the source and target substances consist of the same chromophore with the only difference being the salt form. Please see section 13 for attached justification document.
Reason / purpose for cross-reference:
read-across source
Key result
Decomposition:
yes
Decomp. temp.:
> 250 °C
Remarks on result:
other: No melting point found below 400 °C. No melting point was found between -50°C and decomposition.
Conclusions:
The test material CAS 28706-25-4 decomposed at temperatures >250 degrees celsius.
Executive summary:

The test material CAS 28706-25-4 decomposed at temperatures >250 degrees celsius. This result is considered as the key study for this endpoint as the chromophore is identical in both substances with the only difference being the salt form.

Description of key information

Decomposition occurs and therefore a melting point is not determined.

Key value for chemical safety assessment

Additional information