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Please be aware that this old REACH registration data factsheet is no longer maintained; it remains frozen as of 19th May 2023.

The new ECHA CHEM database has been released by ECHA, and it now contains all REACH registration data. There are more details on the transition of ECHA's published data to ECHA CHEM here.

Diss Factsheets

Administrative data

Endpoint:
melting point/freezing point
Type of information:
experimental study
Adequacy of study:
key study
Study period:
2016
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
test procedure in accordance with national standard methods

Data source

Reference
Reference Type:
study report
Title:
Unnamed
Year:
2016
Report date:
2016

Materials and methods

Test guideline
Qualifier:
according to guideline
Guideline:
other: company SOP
Principles of method if other than guideline:
determination of the melting point by DSC
GLP compliance:
no
Type of method:
differential scanning calorimetry

Test material

Constituent 1
Chemical structure
Reference substance name:
3-hydroxy-3'-nitro-2-naphthanilide
EC Number:
205-209-2
EC Name:
3-hydroxy-3'-nitro-2-naphthanilide
Cas Number:
135-65-9
Molecular formula:
C17H12N2O4
IUPAC Name:
3-hydroxy-N-(3-nitrophenyl)-2-naphthamide

Results and discussion

Melting / freezing point
Melting / freezing pt.:
249 °C
Atm. press.:
ca. 1 atm
Decomposition:
yes
Decomp. temp.:
265 °C
Sublimation:
no

Applicant's summary and conclusion

Conclusions:
The melting point of the substance is 249°C.
Executive summary:

The melting point of the substance was determined by DSC using a Mettler Toledo DSC 823e calorimeter. The heating range was 25- 400 °C, the heating rate was 10 K/min and a aluminum pale with hole was used. The melting point was found to be 249°C; at 265° C the substance started to decompose.