Registration Dossier
Registration Dossier
Please be aware that this old REACH registration data factsheet is no longer maintained; it remains frozen as of 19th May 2023.
The new ECHA CHEM database has been released by ECHA, and it now contains all REACH registration data. There are more details on the transition of ECHA's published data to ECHA CHEM here.
Use of this information is subject to copyright laws and may require the permission of the owner of the information, as described in the ECHA Legal Notice.
EC number: 814-233-8 | CAS number: 444649-70-1
Boiling point
Administrative data
Link to relevant study record(s)
- Endpoint:
- boiling point
- Type of information:
- experimental study
- Adequacy of study:
- key study
- Study period:
- 2011
- Reliability:
- 2 (reliable with restrictions)
- Rationale for reliability incl. deficiencies:
- guideline study without detailed documentation
- Qualifier:
- according to guideline
- Guideline:
- other: conventional differential scanning calorimetry (DSC)
- Principles of method if other than guideline:
- The point where a liquid starts to boil is not readily measured by DSC and depends strongly on the experimental conditions. Hence, it is preferable to refer to the onset of evaporation for a given set of experimental conditions. For temperature-sensitive resins such as acrylate resins, polymerization may occur along with or before evaporation and often prevents proper determination of the evaporation point. As the resins are liquid at room temperature, evaporation is measured at supra-ambient temperatures using conventional differential scanning calorimetry (DSC).
- GLP compliance:
- not specified
- Type of method:
- differential scanning calorimetry
- Specific details on test material used for the study:
- Batch no.: lot # JBGJ0045R
- Key result
- Boiling pt.:
- 183 °C
- Atm. press.:
- ca. 101.3 kPa
- Conclusions:
- Under the study conditions, the boiling point of the test substance was determined to be 183°C (DSC).
- Executive summary:
A study was conducted to determine the boiling point of the test substance according to the conventional differential scanning calorimetry (DSC). A sample of ca. 10 mg was loaded in a standard aluminum crucible (40 µL) fitted with a pierced lid. The measurements were conducted at a linear heating rate of 10°C min-1 using commercial DSC equipment (Mettler DSC823e or Q10 from TA Instruments). The DSC cell was flushed with nitrogen gas at a flow rate of 50 mL min-1. Under the study conditions, the boiling point of the test substance was determined to be 183°C (Herssens, 2011).
Reference
Description of key information
The boiling point was determined according to the conventional differential scanning calorimetry (DSC) (Herssens, 2011)
Key value for chemical safety assessment
- Boiling point at 101 325 Pa:
- 183 °C
Additional information
Information on Registered Substances comes from registration dossiers which have been assigned a registration number. The assignment of a registration number does however not guarantee that the information in the dossier is correct or that the dossier is compliant with Regulation (EC) No 1907/2006 (the REACH Regulation). This information has not been reviewed or verified by the Agency or any other authority. The content is subject to change without prior notice.
Reproduction or further distribution of this information may be subject to copyright protection. Use of the information without obtaining the permission from the owner(s) of the respective information might violate the rights of the owner.
