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Diss Factsheets

Physical & Chemical properties

Melting point / freezing point

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Administrative data

Endpoint:
melting point/freezing point
Type of information:
experimental study
Adequacy of study:
key study
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
guideline study

Data source

Reference
Reference Type:
study report
Title:
Unnamed
Year:
2019
Report date:
2019

Materials and methods

Test guidelineopen allclose all
Qualifier:
according to guideline
Guideline:
EU Method A.1 (Melting / Freezing Temperature)
Qualifier:
according to guideline
Guideline:
OECD Guideline 102 (Melting point / Melting Range)
GLP compliance:
yes (incl. QA statement)
Type of method:
differential scanning calorimetry

Test material

Constituent 1
Chemical structure
Reference substance name:
3,7-dinitroso-1,3,5,7-tetraazabicyclo[3.3.1]nonane
EC Number:
202-928-3
EC Name:
3,7-dinitroso-1,3,5,7-tetraazabicyclo[3.3.1]nonane
Cas Number:
101-25-7
Molecular formula:
C5H10N6O2
IUPAC Name:
3,7-dinitroso-1,3,5,7-tetraazabicyclo[3.3.1]nonane
Test material form:
solid

Results and discussion

Melting / freezing point
Key result
Melting / freezing pt.:
86 °C
Atm. press.:
101 325 Pa
Remarks on result:
other:
Remarks:
The test item 3,7-Dinitroso-1,3,5,7-tetraaza-bicyclo[3.3.1]nonane shows an endothermal effect (combination of boiling and melting) in the 1st and 2nd heating run at 86°C onset temperature (at ambient temperature the sample is a solid). The cooling run shows no crystallization, therefore a cold crystallization is visible during heating in the 2nd heating run.

Applicant's summary and conclusion

Conclusions:
The test item 3,7-Dinitroso-1,3,5,7-tetraaza-bicyclo[3.3.1]nonane shows an endothermal effect (combination of boiling and melting) in the 1st and 2nd heating run at 86°C onset temperature (at ambient temperature the sample is a solid).
The cooling run shows no crystallization, therefore a cold crystallization is visible during heating in the 2nd heating run