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Please be aware that this old REACH registration data factsheet is no longer maintained; it remains frozen as of 19th May 2023.

The new ECHA CHEM database has been released by ECHA, and it now contains all REACH registration data. There are more details on the transition of ECHA's published data to ECHA CHEM here.

Diss Factsheets

Physical & Chemical properties

Melting point / freezing point

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Administrative data

Endpoint:
melting point/freezing point
Type of information:
experimental study
Adequacy of study:
key study
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
other: Test conducted according to internationally accepted testing guidelines.

Data source

Reference
Reference Type:
study report
Title:
Unnamed
Year:
2015
Report date:
2015

Materials and methods

Test guideline
Qualifier:
according to guideline
Guideline:
OECD Guideline 102 (Melting point / Melting Range)
GLP compliance:
no
Type of method:
thermal analysis
Remarks:
DSC

Test material

Constituent 1
Chemical structure
Reference substance name:
2,2'-[[5-acetamido-4-[(2-bromo-4,6-dinitrophenyl)azo]-2-methoxyphenyl]imino]diethyl diacetate
EC Number:
222-813-1
EC Name:
2,2'-[[5-acetamido-4-[(2-bromo-4,6-dinitrophenyl)azo]-2-methoxyphenyl]imino]diethyl diacetate
Cas Number:
3618-72-2
Molecular formula:
C23H25BrN6O10
IUPAC Name:
2-{[2-(acetyloxy)ethyl]({4-[ (E)-2-(2-bromo-4,6-dinitrophenyl)diazen-1-yl]-5acetamido-2-methoxyphenyl})amino}ethyl acetate
Test material form:
solid: particulate/powder

Results and discussion

Melting / freezing point
Atm. press.:
ca. 1 atm
Decomposition:
yes
Decomp. temp.:
ca. 215.9 °C

Any other information on results incl. tables

An endothermic peak was observed between 115 -148 °C, followed by substance decomposition between 216 -353 °C. The decomposition onset is 215.9 °C with an enthalpy energy of 489.9 J/g

Applicant's summary and conclusion

Conclusions:
The substace melting point was determined by DSC according to OECD 102. The decomposition of the substance was observed with onset temperature equal to 215.9 °C.
Executive summary:

The substance melting point was tested by thermoanalysis (DSC) according to OECD 102.

An endothermic peak was observed between 115 -148 °C, followed by substance decomposition between 216 -353 °C. The decomposition onset is 215.9 °C with an enthalpy energy of 489.9 J/g