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Please be aware that this old REACH registration data factsheet is no longer maintained; it remains frozen as of 19th May 2023.

The new ECHA CHEM database has been released by ECHA, and it now contains all REACH registration data. There are more details on the transition of ECHA's published data to ECHA CHEM here.

Diss Factsheets

Physical & Chemical properties

Melting point / freezing point

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Administrative data

Link to relevant study record(s)

Reference
Endpoint:
melting point/freezing point
Type of information:
experimental study
Adequacy of study:
key study
Study period:
23 January - 25 March, 2015
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
guideline study
Remarks:
The study was conducted according to an internationally recognised method, and under GLP. No deviation was reported. Test substance is adequately specified with isomer purity. Therefore full validation applies.
Qualifier:
according to guideline
Guideline:
OECD Guideline 102 (Melting point / Melting Range)
Deviations:
no
Qualifier:
according to guideline
Guideline:
EU Method A.1 (Melting / Freezing Temperature)
Deviations:
no
Principles of method if other than guideline:
Not applicable
GLP compliance:
yes (incl. QA statement)
Remarks:
UK GLP compliance programme (inspected on 05 February 2014 / signed on 07 October 2015
Type of method:
method to determine freezing temperature
Key result
Melting / freezing pt.:
-15 °C

A consistent freezing point value for test item is -15.0 °C (mean of the two replicates -15.0 and -15.0°C) as indicated by a plateau region in the cooling curve at this temperature.

Executive summary:

The freezing point of the test item was determined under GLP according to OECD 102 / EU A1 guideline, freezing point method. Two runs were performed.

A consistent freezing point value for test item is -15.0 °C (mean of the two replicates -15.0 and -15.0 °C) as indicated by a plateau region in the cooling curve at this temperature.

The freezing temperature of the test item has been determined to be -15 °C.

Description of key information

Freezing (i.e. liquid-solid transition) occurs at the temperature of -15°C.

Key value for chemical safety assessment

Melting / freezing point at 101 325 Pa:
-15 °C

Additional information

A fully reliable experimental study, conducted according to a recognized OECD/EU method, is available. It is considered as a key study. The result is retained as key data.