Registration Dossier

Data platform availability banner - registered substances factsheets

Please be aware that this old REACH registration data factsheet is no longer maintained; it remains frozen as of 19th May 2023.

The new ECHA CHEM database has been released by ECHA, and it now contains all REACH registration data. There are more details on the transition of ECHA's published data to ECHA CHEM here.

Diss Factsheets

Administrative data

Endpoint:
melting point/freezing point
Type of information:
experimental study
Adequacy of study:
key study
Study period:
Testing was conducted between 29 April 2009 and 17 June 2009.
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
other: Study conducted in compliance with agreed protocols, with no or minor deviations from standard test guidelines and/or minor methodological deficiencies, which do not affect the quality of the relevant results.

Data source

Reference
Reference Type:
study report
Title:
Unnamed
Year:
2009

Materials and methods

Test guideline
Qualifier:
according to guideline
Guideline:
EU Method A.1 (Melting / Freezing Temperature)
Deviations:
no
GLP compliance:
yes (incl. QA statement)
Remarks:
Date of inspection: 18/08/08 Date of signature: 04/03/09
Type of method:
other: differential scanning calorimetry

Test material

Constituent 1
Chemical structure
Reference substance name:
3-{[1,1'-biphenyl]-4-yl}-6-(4-chlorophenyl)-1H,2H,4H,5H-pyrrolo[3,4-c]pyrrole-1,4-dione
EC Number:
700-341-1
Cas Number:
105194-34-1
Molecular formula:
C24H15ClN2O2
IUPAC Name:
3-{[1,1'-biphenyl]-4-yl}-6-(4-chlorophenyl)-1H,2H,4H,5H-pyrrolo[3,4-c]pyrrole-1,4-dione
Constituent 2
Reference substance name:
3-(biphenyl-4-yl)-6-(4-chlorophenyl)-2,5-dihydropyrrolo[3,4-c]pyrrole-1,4-dione
IUPAC Name:
3-(biphenyl-4-yl)-6-(4-chlorophenyl)-2,5-dihydropyrrolo[3,4-c]pyrrole-1,4-dione
Details on test material:
Sponsor's identification : PDE-28
Description : red powder
Purity : 97%
Batch number : 1RF-8017
Date received : 23 March 2009
Storage conditions : room temperature, in the dark

Results and discussion

Melting / freezing point
Melting / freezing pt.:
> 400 °C

Any other information on results incl. tables

The absence of any significant thermal events and the unchanged physical state/appearance of the test material residue on completion of each determination confirmed that no phase transition occurred. Therefore the melting temperature of the test material was greater than 400°C, >673 K.

Applicant's summary and conclusion

Conclusions:
The melting/freezing temperature of the test material has been determined to be greater than 673 K.
Executive summary:

Melting/Freezing Temperature:

Greater than 673 K, by differential scanning caloritry, using ASTM E537-86, Method A1 Melting/Freezing Temperature of Commission Regulation (EC) No 440/2008 of 30 May 2008.