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Please be aware that this old REACH registration data factsheet is no longer maintained; it remains frozen as of 19th May 2023.

The new ECHA CHEM database has been released by ECHA, and it now contains all REACH registration data. There are more details on the transition of ECHA's published data to ECHA CHEM here.

Diss Factsheets

Administrative data

Endpoint:
melting point/freezing point
Type of information:
experimental study
Adequacy of study:
key study
Study period:
2010
Reliability:
1 (reliable without restriction)

Data source

Reference
Reference Type:
study report
Title:
Unnamed
Year:
2010
Report date:
2010

Materials and methods

Test guideline
Qualifier:
according to guideline
Guideline:
other: Analytical method DSC, SOP: EQH-1020-AA-0007 (25-160 °C, 10 K/min, aluminium pan), Apparatus Mettler Toledo, DSC 823e
Deviations:
not specified
Principles of method if other than guideline:
Analytical method: DSC
SOP: EQH-1020-AA-0007 (25-160 °C, 10 K/min, aluminium pan)
Apparatus: Mettler Toledo, DSC 823e
Documentation: 08-33369 (03.03.2008)
GLP compliance:
not specified
Type of method:
other: Differential scanning calorimetry

Test material

Constituent 1
Chemical structure
Reference substance name:
o-phenylenediamine
EC Number:
202-430-6
EC Name:
o-phenylenediamine
Cas Number:
95-54-5
Molecular formula:
C6H8N2
IUPAC Name:
benzene-1,2-diamine

Results and discussion

Melting / freezing point
Melting / freezing pt.:
101 °C
Atm. press.:
ca. 1 atm
Decomposition:
yes
Decomp. temp.:
323 °C
Remarks on result:
other: decomposition in the sealed vial at 323 °C with a mean energy of at least 870 J/g.

Applicant's summary and conclusion

Conclusions:
The melting point of the test item determined by DSC is 101 °C.
Executive summary:

The melting point of the test item determined by DSC is 101 °C.