Registration Dossier
Registration Dossier
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EC number: 300-947-2 | CAS number: 93964-99-9
Auto flammability
Administrative data
- Endpoint:
- auto-ignition temperature (liquids)
- Type of information:
- experimental study
- Adequacy of study:
- key study
- Study period:
- Experimental starting date: 12 June 2016 Experimental completion date: 01 July 2016
- Reliability:
- 1 (reliable without restriction)
Data source
Reference
- Reference Type:
- study report
- Title:
- Unnamed
- Year:
- 2 016
- Report date:
- 2016
Materials and methods
Test guideline
- Qualifier:
- according to guideline
- Guideline:
- EU Method A.15 (Auto-Ignition Temperature (Liquids and Gases))
- GLP compliance:
- yes
Test material
- Reference substance name:
- O,O-dibutyl hydrogen thiophosphate, compound with 1-octylamine (1:1)
- EC Number:
- 300-947-2
- EC Name:
- O,O-dibutyl hydrogen thiophosphate, compound with 1-octylamine (1:1)
- Cas Number:
- 93964-99-9
- Molecular formula:
- C8H19N.C8H19O3PS
- IUPAC Name:
- octan-1-amine dibutyl sulfanylphosphonate
- Reference substance name:
- Octylamine
- EC Number:
- 203-916-0
- EC Name:
- Octylamine
- Cas Number:
- 111-86-4
- Molecular formula:
- C8H19N
- IUPAC Name:
- octan-1-amine
- Test material form:
- liquid
Constituent 1
impurity 1
- Specific details on test material used for the study:
- Information as provided by the Sponsor. The Certificate of Analysis provided by the Sponsor is presented as Annex 2 (Please see Attachment Section of this Summary).
Identification: X-19575 Phosphorothioic acid, O,O-dibutyl ester, compd. with 1-octanamine, CASRN 93964-99-9
Appearance/Physical state: amber colored viscous liquid
Batch: X-019575-00-00
Purity: UVCB Substance (treat as 100%)
Expiry date: 01 June 2017
Storage conditions: room temperature, in the dark
Results and discussion
Auto-ignition temperature (liquids / gases)
- Auto-ignition temperature:
- 314 °C
- Atm. press.:
- >= 99.8 - <= 100.4 kPa
Any other information on results incl. tables
Results
Results of the auto-ignition temperature determination are shown in the following table:
Table 5
Test Temperature (ºC) |
Sample Volume (µL) |
Ignition Delay (s) |
Observations |
200 (clean flask) |
70 |
>300 |
No ignition. |
250 (clean flask) |
70 |
>300 |
No ignition. Grey fumes were emitted. |
300 (clean flask) |
70 |
>300 |
No ignition. Grey fumes were emitted. |
350 |
70 |
6 |
An orange flame. Grey fumes were emitted. |
340 |
70 |
10 |
An orange flame. Grey fumes were emitted. |
330 |
70 |
16 |
An orange flame. Grey fumes were emitted. |
320 |
70 |
20 |
An orange flame. Grey fumes were emitted. |
310 |
70 |
>300 |
No ignition. Grey fumes were emitted. |
312 (clean flask) |
70 |
>300 |
No ignition. Grey fumes were emitted. |
314 (clean flask) |
70 |
>300 |
No ignition. Grey fumes were emitted. |
316 (clean flask) |
70 |
>300 |
No ignition. Grey fumes were emitted. |
318 (clean flask) |
70 |
24 |
An orange flame. Grey fumes were emitted. |
316 (clean flask) |
200 |
>300 |
No ignition. Grey fumes were emitted. |
316 (clean flask) |
400 |
16 |
An orange flame. Grey fumes were emitted. |
314 (clean flask) |
400 |
>300 |
No ignition. Grey fumes were emitted. |
314 (clean flask) |
600 |
>300 |
No ignition. Grey fumes were emitted. |
314 (clean flask) |
800 |
>300 |
No ignition. Grey fumes were emitted. |
314 (clean flask) |
1000 |
42 |
An orange flame. Grey fumes were emitted. |
312 (clean flask) |
1000 |
>300 |
No ignition. Grey fumes were emitted. |
312 (clean flask) |
1200 |
>300 |
No ignition. Grey fumes were emitted. |
312 (clean flask) |
1400 |
>300 |
No ignition. Grey fumes were emitted. |
312 (clean flask) |
1600 |
>300 |
No ignition. Grey fumes were emitted. |
312 (clean flask) |
1800 |
>300 |
No ignition. Grey fumes were emitted. |
Room temperature: 20 to 21 °C
Atmospheric pressure: 99.8 to 100.4 kPa
Applicant's summary and conclusion
- Conclusions:
- The test item has been determined to have an auto-ignition temperature of 314 ± 5 °C.
- Executive summary:
The determination was carried out using a procedure*designed to be compatible with Method A.15 Auto-Ignition Temperature (Liquids and Gases) of Commission Regulation (EC) No 440/2008 of 30 May 2008.
*Based on, Anon (1987), 70Electrical Apparatus for Explosive Gas Atmospheres. Part 4: Method of Test for Ignition Temperature. IEC Publications79-4,P1-19.
Conclusion
The test item has been determined to have an auto-ignition temperature of 314 ± 5 °C.
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