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Diss Factsheets

Physical & Chemical properties

Melting point / freezing point

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Administrative data

Link to relevant study record(s)

Reference
Endpoint:
melting point/freezing point
Type of information:
experimental study
Adequacy of study:
key study
Study period:
October 07, 2014
Reliability:
2 (reliable with restrictions)
Rationale for reliability incl. deficiencies:
guideline study with acceptable restrictions
Qualifier:
according to guideline
Guideline:
OECD Guideline 102 (Melting point / Melting Range)
Principles of method if other than guideline:
SOP - STR 028
GLP compliance:
no
Type of method:
thermal analysis
Melting / freezing pt.:
> 440 °C
Conclusions:
The test substance was analyzed in accordance with OECD test guidelines 102 and 103. Under the reported experimental conditions no melting point at temperature below 440°C.
Executive summary:

Method


Differential Scanning Calorimetry (DSC) according to the OECD Test Guidelines 102 and 103.


 


Results


Between 40 and 180 °C there is a release of imbibition/crystallisation water, followed by three endothermic effect: the first between 238 -259 °C (onset = 242.9 °C, enthalpy = - 0.7 J/g), the second between 259-299 °C (onset at 269.3 °C, enthalpy = -5.6 J/g) and the third between 299-353 °C (onset at 305.3 °C, enthalpy = - 38.3 J/g).


 


Conclusion


The test item doesn’t melt at temperature below 440 °C.

Description of key information

OECD TG 102 - Thermal analysis - No melting point at temperature below 440 °C.

Key value for chemical safety assessment

Additional information