Registration Dossier
Registration Dossier
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EC number: - | CAS number: -
Auto flammability
Administrative data
Link to relevant study record(s)
- Endpoint:
- auto-ignition temperature (liquids)
- Type of information:
- experimental study
- Adequacy of study:
- key study
- Study period:
- 15 March 2017 to 22 March 2017
- Reliability:
- 1 (reliable without restriction)
- Rationale for reliability incl. deficiencies:
- guideline study
- Qualifier:
- according to guideline
- Guideline:
- EU Method A.15 (Auto-Ignition Temperature (Liquids and Gases))
- Deviations:
- no
- GLP compliance:
- yes (incl. QA statement)
- Key result
- Auto-ignition temperature:
- 372 °C
- Atm. press.:
- >= 99 - <= 101 kPa
- Conclusions:
- The test item was determined to have an autoignition temperature of 372 ± 5 °C at 99 to 101 kPa.
- Executive summary:
GUIDELINE
The determination was carried out using a Carbolite flask heater and a procedure designed to be compatible with Method A.15 Auto-Ignition Temperature (Liquids and Gases) of Commission Regulation (EC) No 440/2008 of 30 May 2008.
RESULTS
The test item was determined to have an autoignition temperature of 372 ± 5 °C at 99 to 101 kPa.
Reference
TABLE 2 - RESULTS OF THE AUTO–IGNITION TEMPERATURE DETERMINATION
Test temperature (°C) |
Volume (µL) |
Ignition delay (s) |
Observations |
200 (clean flask) |
70 |
> 300 |
No ignition. Grey fumes emitted. |
250 (clean flask) |
70 |
> 300 |
No ignition. Grey fumes emitted. |
300 (clean flask) |
70 |
> 300 |
No ignition. Grey fumes emitted. |
350 |
70 |
> 300 |
No ignition. Grey fumes emitted. |
400 |
70 |
13 |
Orange flame. Grey fumes emitted. |
390 |
70 |
> 300 |
No ignition. Grey fumes emitted. |
398 |
70 |
13 |
Red flame. Grey fumes emitted. |
396 |
70 |
> 300 |
No ignition. Grey fumes emitted. |
396 (clean flask) |
70 |
> 300 |
No ignition. Grey fumes emitted. |
396 (clean flask) |
200 |
> 300 |
No ignition. Grey fumes emitted. |
396 (clean flask) |
400 |
> 300 |
No ignition. Grey fumes emitted. |
396 (clean flask) |
600 |
> 300 |
No ignition. Grey fumes emitted. |
396 (clean flask) |
800 |
> 300 |
No ignition. Grey fumes emitted. |
396 (clean flask) |
1000 |
116 |
Red flame. Grey fumes emitted. |
394 (clean flask) |
1000 |
> 300 |
No ignition. Grey fumes emitted. |
394 (clean flask) |
1200 |
> 300 |
No ignition. Grey fumes emitted. |
394 (clean flask) |
1400 |
> 300 |
No ignition. Grey fumes emitted. |
394 (clean flask) |
1600 |
162 |
Red flame. Grey fumes emitted. |
392 (clean flask) |
1600 |
> 300 |
No ignition. Grey fumes emitted. |
392 (clean flask) |
1800 |
> 300 |
No ignition. Grey fumes emitted. |
392 (clean flask) |
2000 |
> 300 |
No ignition. Grey fumes emitted. |
392 (clean flask) |
2200 |
> 300 |
No ignition. Grey fumes emitted. |
392 (clean flask) |
2400 |
132 |
Orange-red flame. Grey fumes emitted. |
390 (clean flask) |
2400 |
118 |
Orange-red flame. Grey fumes emitted. |
388 (clean flask) |
2400 |
177 |
Orange-red flame. Grey fumes emitted. |
386 (clean flask) |
2400 |
203 |
Orange-red flame. Grey fumes emitted. |
384 (clean flask) |
2400 |
213 |
Orange-red flame. Grey fumes emitted. |
382 (clean flask) |
2400 |
245 |
Orange-red flame. Grey fumes emitted. |
380 (clean flask) |
2400 |
> 300 |
No ignition. Grey fumes emitted. |
380 (clean flask) |
2600 |
> 300 |
No ignition. Grey fumes emitted. |
380 (clean flask) |
2800 |
> 300 |
No ignition. Grey fumes emitted. |
380 (clean flask) |
3000 |
213 |
No ignition. Grey fumes emitted. |
378 (clean flask) |
3000 |
186 |
Red flame. Grey fumes emitted. |
376 (clean flask) |
3000 |
> 300 |
No ignition. Grey fumes emitted. |
376 (clean flask) |
3200 |
> 300 |
No ignition. Grey fumes emitted. |
376 (clean flask) |
3400 |
> 300 |
No ignition. Grey fumes emitted. |
376 (clean flask) |
3600 |
270 |
Red flame. Grey fumes emitted. |
374 (clean flask) |
3600 |
> 300 |
No ignition. Grey fumes emitted. |
374 (clean flask) |
3800 |
272 |
Red flame. Grey fumes emitted. |
372 (clean flask) |
3800 |
284 |
Red flame. Grey fumes emitted. |
370 (clean flask) |
3800 |
> 300 |
No ignition. Grey fumes emitted. |
370 (clean flask) |
4000 |
> 300 |
No ignition. Grey fumes emitted. |
370 (clean flask) |
4200 |
> 300 |
No ignition. Grey/brown fumes emitted. |
370 (clean flask) |
4400 |
> 300 |
No ignition. Grey/brown fumes emitted. |
370 (clean flask) |
4600 |
> 300 |
No ignition. Grey/brown fumes emitted. |
Room temperature: 23 to 24 °C
Atmospheric pressure: 99 to 101 kPa
Observed result: 372 ± 5 °C
Description of key information
The test item was determined to have an autoignition temperature of 372 ± 5 °C at 99 to 101 kPa.
Key value for chemical safety assessment
- Autoflammability / Self-ignition temperature at 101 325 Pa:
- 372 °C
Additional information
GUIDELINE
The determination was carried out using a Carbolite flask heater and a procedure designed to be compatible with Method A.15 Auto-Ignition Temperature (Liquids and Gases) of Commission Regulation (EC) No 440/2008 of 30 May 2008.
RESULTS
The test item was determined to have an autoignition temperature of 372 ± 5 °C at 99 to 101 kPa.
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