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Diss Factsheets

Physical & Chemical properties

Melting point / freezing point

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Administrative data

Link to relevant study record(s)

Reference
Endpoint:
melting point/freezing point
Type of information:
experimental study
Adequacy of study:
key study
Study period:
2006-11-23 to 2007-01-17
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
guideline study
Qualifier:
according to guideline
Guideline:
OECD Guideline 102 (Melting point / Melting Range)
Version / remarks:
1995
Deviations:
no
Qualifier:
according to guideline
Guideline:
EU Method A.1 (Melting / Freezing Temperature)
Version / remarks:
92/69/EEC
Deviations:
no
GLP compliance:
yes (incl. QA statement)
Type of method:
differential scanning calorimetry
Key result
Melting / freezing pt.:
8 °C
Atm. press.:
1 013.3 hPa
Decomposition:
no
Sublimation:
no

Four DSC-runs in aluminium crucibles with a hole showed an endothermic effect in the temperature

range of 2 - 30°C with an onset temperature of about 7 - 8 °C. The onset temperature is derived

from the intersection of the tangent line with the highest slope of the endothermic peak with the

baseline.

The test item has a melting point of 8 °C.

Ident-No.

Onset / °C

Temperature range / °C

25012

8.10

2-30

25025

8.38

5-30

25027

7.18

4-24

25028

7.26

2-30

Conclusions:
The mean melting temperature of the test item is 8 °C.
Executive summary:

The melting point of the test item was determined according to OECD test guideline 102 and Council Directive 92/69/EEC, Method A.1. Four DSC-runs in aluminium crucibles with a hole showed an endothermic effect in the temperature range of 2 - 30°C with an onset temperature of about 7 - 8 °C. The onset temperature is derived from the intersection of the tangent line with the highest slope of the endothermic peak with the baseline. Accordingly, the mean melting temperature of the test item was determined to be 8 °C.

Description of key information

The mean melting temperature of the test item is 8 °C (reference 4.2-1).

Key value for chemical safety assessment

Melting / freezing point at 101 325 Pa:
8 °C

Additional information

The melting point of the test item was determined according to OECD test guideline 102 and Council Directive 92/69/EEC, Method A.1. Four DSC-runs in aluminium crucibles with a hole showed an endothermic effect in the temperature range of 2 - 30°C with an onset temperature of about 7 - 8 °C. The onset temperature is derived from the intersection of the tangent line with the highest slope of the endothermic peak with the baseline. Accordingly, the mean melting temperature of the test item was determined to be 8 °C.