Registration Dossier

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Please be aware that this old REACH registration data factsheet is no longer maintained; it remains frozen as of 19th May 2023.

The new ECHA CHEM database has been released by ECHA, and it now contains all REACH registration data. There are more details on the transition of ECHA's published data to ECHA CHEM here.

Diss Factsheets

Administrative data

Endpoint:
thermal stability
Type of information:
experimental study
Adequacy of study:
weight of evidence
Reliability:
2 (reliable with restrictions)
Rationale for reliability incl. deficiencies:
study well documented, meets generally accepted scientific principles, acceptable for assessment

Data source

Reference
Reference Type:
study report
Title:
Unnamed
Year:
1994
Report date:
1994

Materials and methods

Test guideline
Qualifier:
according to guideline
Guideline:
other: VDI 2263 Part 1
Principles of method if other than guideline:
Storage stability
GLP compliance:
no

Test material

Constituent 1
Reference substance name:
Acid Blue 193
IUPAC Name:
Acid Blue 193

Results and discussion

Any other information on results incl. tables

Storage stability

The test substance showed a temperature rise of 7 K, at a storage temperature of 150 °C. The maximum was reached after 2.75 hours. Drying at a maximum temperature of 150 °C with a maximum residence time of 120 hours is possible if it is ensured that the temperature of 150 °C can not be exceeded.

Storage temperature Amout Exotherm reaction after storage of Time after maximum reaction Maximum temperature during the exothermy Appearance of the sample
170 °C 400 ml Directly 4.25 h 669 °C White residue
160 °C 400 ml Directly 3 h 175 °C Unchanged
150 °C 400 ml Directly 2.75 h 157 °C Unchanged

Applicant's summary and conclusion

Conclusions:
The test substance showed a temperature rise of 7 K, at a storage temperature of 150 °C. The maximum was reached after 2.75 hours. Drying at a maximum temperature of 150 °C with a maximum residence time of 120 hours is possible if it is ensured that the temperature of 150 °C can not be exceeded.
Executive summary:

Storage stability was assessed in accordance with VDI 2263 Part 1. 400 ml of the substance sample were placed in a wire mesh basket under air flow of 100 l/h.

The sample temperature was measured using two thermocouples (sample center and side). The reference temperature was a thermocouple in the gas space of the furnace. All temperature values were recorded by computer system.

The test substance showed a temperature rise of 7 K, at a storage temperature of 150 °C. The maximum was reached after 2.75 hours. Drying at a maximum temperature of 150 °C with a maximum residence time of 120 hours is possible if it is ensured that the temperature of 150 °C can not be exceeded.