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Diss Factsheets

Physical & Chemical properties

Melting point / freezing point

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Reference
Endpoint:
melting point/freezing point
Type of information:
experimental study
Adequacy of study:
key study
Study period:
2015-12-01
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
guideline study
Qualifier:
according to guideline
Guideline:
EU Method A.1 (Melting / Freezing Temperature)
Version / remarks:
2008
Deviations:
no
Qualifier:
according to guideline
Guideline:
OECD Guideline 102 (Melting point / Melting Range)
Version / remarks:
1995
Deviations:
no
GLP compliance:
yes
Type of method:
capillary method
Key result
Decomposition:
yes
Remarks:
The melted substance appeared brown, indicating decomposition at about 260 °C.
Decomp. temp.:
ca. 260 °C
Sublimation:
no

Decomposition of the test item was determined to start at 260 °C. An effect similiar to melting was observed at 281.6 °C.


Results of individual measurements: 281.2; 282.2; 281.4 °C (standard deviation of 0.53)

Conclusions:
The test item melts under decomposition at 281.6 °C.
Executive summary:

The melting point of the registered substance was determined in an experimental study under GLP conditions according to OECD Test Guideline 102.


The determination of the melting temperature of the test substance was performed by the capillary method with hot block heating.


Decomposition of the test item was determined to start at 260 °C. An effect similiar to melting was observed at 281.6 °C.

Description of key information

The test item decomposed starting at 260 °C (reference 4.2-1).

Key value for chemical safety assessment

Additional information

The melting point of the substance was determined in an experimental study under GLP conditions according to OECD Test Guideline 102. The test item started decomposition at approximately 260 °C. Decomposition was indicated by a change in the substance's colour. An effect similar to melting was detected at 281.6 °C.