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Please be aware that this old REACH registration data factsheet is no longer maintained; it remains frozen as of 19th May 2023.

The new ECHA CHEM database has been released by ECHA, and it now contains all REACH registration data. There are more details on the transition of ECHA's published data to ECHA CHEM here.

Diss Factsheets

Administrative data

Endpoint:
nanomaterial porosity
Type of information:
experimental study
Adequacy of study:
key study
Study period:
02-11 April 2018

Data source

Reference
Reference Type:
study report
Title:
Unnamed
Year:
2018
Report date:
2018

Materials and methods

GLP compliance:
no
Remarks:
but study conducted in a laboratory holding a current statement of GLP compliance.
Type of method:
BET
Details on methods and data evaluation:
Methodology
The test substance, titanium nitride, was conditioned for 16 hours at 40 °C, with a Nitrogen gas purge, cooled and then run on the Porosimeter.

Full isothermal analysis (porosity) was performed using Barrett-Joyner-Halenda (BJH) method with relative pressure (P/Po) range of 0.05 up to 1.00 followed by desorption back down to a relative pressure of 0.06.

Duplicated analysis was performed.

Test material

Constituent 1
Chemical structure
Reference substance name:
Titanium nitride
EC Number:
247-117-5
EC Name:
Titanium nitride
Cas Number:
25583-20-4
Molecular formula:
NTi
IUPAC Name:
titanium nitride
Test material form:
solid: nanoform
Specific details on test material used for the study:
Weights taken: Weight 1: 03553g
Weight 2: 0.4253g

Data gathering

Instruments:
Micromeritics Tristar II 3020 Porosimeter with SmartPrep 065, LIMS 2214, SOP 099.02/2

Results and discussion

Specific pore volume
Key result
Mean:
0.05 cm³/g
Modal pore diameter
Key result
Mean:
80.4 other: Å

Applicant's summary and conclusion

Conclusions:
The mean pore size of Ti, measured with a porosimeter, is 80.4 Å.