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Please be aware that this old REACH registration data factsheet is no longer maintained; it remains frozen as of 19th May 2023.

The new ECHA CHEM database has been released by ECHA, and it now contains all REACH registration data. There are more details on the transition of ECHA's published data to ECHA CHEM here.

Diss Factsheets

Administrative data

Endpoint:
boiling point
Type of information:
experimental study
Adequacy of study:
key study
Study period:
Testing was conducted between 14 February 2008 and 31 March 2008.
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
other: Study conducted in compliance with agreed protocols, with no or minor deviations from standard test guidelines and/or minor methodological deficiencies, which do not affect the quality of relevant results.

Data source

Reference
Reference Type:
study report
Title:
Unnamed
Year:
2008
Report date:
2008

Materials and methods

Test guideline
Qualifier:
according to guideline
Guideline:
EU Method A.2 (Boiling Temperature)
Deviations:
no
GLP compliance:
yes (incl. QA statement)
Remarks:
The work described was performed in compliance with UK GLP standards (Schedule 1, Good Laboratory Practice Regulations 1999 (SI 1999/3106 as amended by SI 2004/0994)). Date of inspection: 21/08/2007. Date of signature: 23/04/2008
Type of method:
differential scanning calorimetry

Test material

Constituent 1
Details on test material:
Sponsor's identification :Hatcol 1760
Description : clear colourless slightly viscous liquid
Purity : >99%
Date received : 04 February 2008
Storage conditions :room temperature, in the dark

Results and discussion

Boiling point
Boiling pt.:
679 K
Atm. press.:
104.54 kPa
Decomposition:
ambiguous
Remarks:
See comments in "Remarks on results" section

Any other information on results incl. tables

On completion of the tests the crucible lids were removed. This revealed a yellow liquid residue. This was most likely the larger components of the test material that had not yet boiled. As the test material was initially colourless, the yellow colour of the residue may have indicated that some decomposition had occurred, but this was not evident in the thermograms. Therefore, no values for the decomposition can be quoted.

Thermal Event

Interpretation

Temperature

ºC

K

Endotherm

boiling temperature

405.92

679

Atmospheric pressure: 104.54 kPa

Applicant's summary and conclusion

Conclusions:
The test material has been determined to partially boil with decomposition from 679 ± 0.5 K at 104.54 kPa.
Executive summary:

Method

The determination was carried out by differential scanning calorimetry (DSC) using the procedure specified in ASTM E537-86, Method A2 of Commission Directive 92/69/EEC (which constitutes Annex V of Council Directive 67/548/EEC).

Results

The test material has been determined to partially boil with decomposition from 679 ± 0.5 K at 104.54 kPa.