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Reference
Endpoint:
relative self-ignition temperature (solids)
Type of information:
experimental study
Adequacy of study:
key study
Study period:
18 March 2019 to 18 April 2019
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
guideline study
Qualifier:
according to guideline
Guideline:
EU Method A.16 (Relative Self-Ignition Temperature for Solids)
GLP compliance:
yes
Specific details on test material used for the study:
SOURCE OF TEST MATERIAL
- Lot/batch No.of test material: E01255-297
- Expiration date of the lot/batch: 31 December 2022
Key result
Remarks on result:
no self ignition observed under the test conditions

An exothermic effect of the test item by self-heating was observed at an oven temperature of 164 °C. During this effect the test item reached a temperature of 198 °C. According to the guideline, a test item is self-ignitable when the sample temperature reaches 400 °C by self-heating. Based on this, the test item is considered ‘not self-ignitable’.

After the experiment, the test item had turned into a charred residue and was partially collected in a container that was placed below the cube. It indicated that the test item had been partially molten, decomposed and/or reacted during the experiment.

Conclusions:
The self-ignition temperature of the test item was determined using a temperature programmed laboratory oven, a stainless steel wire mesh cube, NiCr/NiAl thermocouples and a temperature recording device. Based on the results obtained the test item is considered ‘not self-ignitable’.
Executive summary:

The study was performed based on procedures in the EU Method A.16 (Relative Self-Ignition Temperature for Solids). The self-ignition temperature of the test item was determined using a temperature programmed laboratory oven, a stainless steel wire mesh cube, NiCr/NiAl thermocouples and a temperature recording device. An exothermic effect of the test item by self-heating was observed at an oven temperature of 164 °C, during this effect the test item reached a temperature of 198 °C. However, according to the guideline, a test item is self-ignitable when the sample temperature reaches 400 °C by self-heating. Based on the results obtained the test item is considered ‘not self-ignitable’.

Description of key information

The study was performed based on procedures in the EU Method A.16 (Relative Self-Ignition Temperature for Solids). The self-ignition temperature of the test item was determined using a temperature programmed laboratory oven, a stainless steel wire mesh cube, NiCr/NiAl thermocouples and a temperature recording device. An exothermic effect of the test item by self-heating was observed at an oven temperature of 164 °C, during this effect the test item reached a temperature of 198 °C. However, according to the guideline, a test item is self-ignitable when the sample temperature reaches 400 °C by self-heating. Based on the results obtained the test item is considered ‘not self-ignitable’.

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