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Physical & Chemical properties

Density

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Administrative data

Link to relevant study record(s)

Reference
Endpoint:
relative density
Type of information:
experimental study
Adequacy of study:
key study
Study period:
2017-07-10 - 2018-03-07
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
guideline study
Reason / purpose for cross-reference:
reference to same study
Reason / purpose for cross-reference:
reference to same study
Reason / purpose for cross-reference:
reference to same study
Reason / purpose for cross-reference:
reference to same study
Qualifier:
according to guideline
Guideline:
OECD Guideline 109 (Density of Liquids and Solids)
Deviations:
no
Qualifier:
according to guideline
Guideline:
EU Method A.3 (Relative Density)
Deviations:
no
GLP compliance:
yes (incl. QA statement)
Remarks:
The department of health of the government of the united kingdom
Type of method:
pycnometer method
Remarks:
gas comparison pycnometer
Specific details on test material used for the study:
Identification: m- & o-terphenyl rxn mass
Appearance/Physical state: a cream colored solid block
Storage conditions: approximately 4 °C, in the dark, under nitrogen
Key result
Type:
relative density
Density:
1.11 other: no unit applicable for rel. density
Temp.:
20 °C

Calibration

 Determination  P1 (psig)  P2 (psig)  P3 (psig)  P4 (psig)  Reference Cell Volume (cm³)  Sample Cell Volume (cm³)
 1  17.347  6.569  17.060  8.453  90.855  149.069
 2  17.050  6.457  17.036  8.442  90.852  149.047
 2  17.014  6.446  17.108

8.481

 90.894

149.018

             Mean

 90.867

 149.045

Sample

The pressure readings and volumes obtained for the vessel and the vessel containing the test item are shown in the following table:

Determination

Test

Vessel

Vessel and Test Item

P1(sample)

(psig)

P2(sample)

(psig)

Volume
(cm3)

P3(sample) (psig) P4(sample) (psig) Volume (cm3)
    1   A 17.073 6.871 14.126 17.196 7.980 44.103
B 17.022 6.847 14.011 17.076 7.923 44.071
C 17.013 6.846 14.098 17.063 7.915 44.022
 2      A 17.008 6.855 14.461 17.106 8.216 50.723
B 17.137 6.903 14.330 17.128 8.226 50.710
C 17.069 6.877 14.376 17.096 8.208 50.650

The calculated mean volumes and densities are shown in the following table:

Determination Mean Volume of Vessel (cm3) Mean Volume of Vessel and Test Item (cm3) Volume of Test Item (cm3) Density (kg/m3)
1 14.078 44.065 29.987 1.11 x 103
2 14.389 50.694 36.305 1.11 x 103

Mean density: 1.11 x 103 kg/m3

Relative density: 1.11

Temperature: 20.0 ± 0.5 ºC

Discussion

Duplicate determinations were performed to ensure a reproducibility of less than ± 20 kg/m3 was obtained.

Conclusion

The density of the test item was determined to be 1.11 x 103 kg/m3 at 20.0 ± 0.5 ºC. The corresponding relative density was calculated to be 1.11.

Conclusions:
The density of the test item was determined to be 1.11 x 10E3 kg/m3 at 20.0 ± 0.5 ºC. The corresponding relative density was calculated to be 1.11.
Executive summary:

The relative density of the test sample was determined to be 1.11 x 103 kg/m3 at 20.0 ± 0.5 ºC; relative density value 1.11, determined according to GLP using a gas comparison pycnometer procedure designed to be compatible with Method A.3 Relative Density of Commission Regulation (EC) No 440/2008 of 30 May 2008 and Method 109 of the OECD Guidelines for Testing of Chemicals, 02 October 2012.

Description of key information

The relative density of the test sample was determined to be 1.11 x 103kg/m3at 20.0 ± 0.5 ºC; relative density value 1.11, determined according to GLP using a gas comparison pycnometer procedure designed to be compatible with Method A.3 Relative Density of Commission Regulation (EC) No 440/2008 of 30 May 2008 and Method 109 of the OECD Guidelines for Testing of Chemicals, 02 October 2012.

Key value for chemical safety assessment

Relative density at 20C:
1.11

Additional information